GC/MS analysis results for sample AD23271, Oct 15 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1201\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Hexanone Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 6.48 1.11 ug/1 111413 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanon^ 100 C6H12O 000591-78-6 91 2 2-Hexanqxie, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 74 3 Methyl sobutyl Ketone 100 C6H12O 000108-10-1 58 4 Oxirap' , 2-methyl-2-(1-methylethyl) 100C6H12Q 072221-03-5 56 <\bundance Scan 157 (6.480 min): 23271 .D (-) m/z 42795 100.00% 43

58 5000

............ rrpjl. 71 , ? ....... . __620_6,40_6W__S80^_ 51 , I ‘ 1' ' ' Wz 58.05 54.36% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 43

58 J 5000 6.20 6.40 6.60 6.80 “m/z 41.05 17767% 27 71 85 100 ........ I ''l ' ' ' I I ' I, , ....I.... I , , , , I.......... T)/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.20 6.40 6.60 6.80 5000 29 m/z 57.00 17.57%

' 1 ' ‘ ' I ' ' ‘ ' I I J. T-p-n-rpr 140 nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63354: Methyl Isobutyl Ketone J 43 6.20 6.40 6.60 6.80 m/z 100.05 12.23%

5000 58 85 100

n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

23271.D NP091101.M Mon Oct 15 09:37:40 2001 Page 2

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