GC/MS analysis results for sample AD23271, Oct 15 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator: 209 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.51 ug/1 51042 1,4-Dichlorobenzene-d4 11.77 Hit# Q 5 Tentative ID MW MolForm CAS# Qual

B 3 exanone tane, 2,2-dimethyl- 100 C6H12O 86 C6H14 000589-38-8 91 000075-83-2 59 3 3-Pentanone, 2-methyl- 100 C6H12O 000565-69-5 53 Heptane, 3,3-dimethyl- 128 C9H20 004032-86-4 42 irtdance Scan 146 (6.379 min): 23271 .D (-) m/z 43700 100.00% 43 57

71 5000 100

6.00 6.20 6.40 6.60 6.80 |nri|iiil| + jirrnTW ............ +TI|llll|IIITj+TITlTni|IIH m/z 57700 91.38% Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63358:3-Hexanone

57

71 5000 6.00 6.20 6.40 6.60 6.80 100 m/z 71.00 59.62% I . I , 85 TTTTyTTTTyrrrqTTT7pTTTpTTTp-rTT]H44+pTTTpTTT-|rH-1pTTT]TTTTyt+TTpTTTpTTTpTrTpTTTJ^^ p ■n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance

5000 29 #62861: Butane, 2,2-dimethyl- 43 517 71 JUJxL 6.00 6.20 m/z 100.0532734% 6.40 6.60 6.80

...... ’h....... I " " I ‘" I iTprrrpTTT p/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63398:3-Pentanone, 2-methyl- \ . .................... (........... . 5(7 6.00 6.20 6.40 6.60 6.80 43 “mTz 41.05 28.14%

5000 100 71 ............ ......... I I..................... II|I?H||| 85 ..... . ‘ I" "I" " I '' I" " I" " I"'' I'' I" " tTTTprrrp p/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

23271.D NP091101.M Mon Oct 15 09:37:38 2001 Page 1

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