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GC/MS analysis report for sample AD25842, Dec 2001

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DEP laboratory report documenting GC/MS results for sample AD25842 analyzed on December 6, 2001.

NYC-WTC_000070154–000070165

Folder label: “GCMS Scan X 10/30/01 An 11/20/01

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Scanned page image, NYC-WTC_000070163
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV1901\25840.D Vial: 7 Acq On : 19 Nov 2001 9:08 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.60 ug/1 114713 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 “entative ID MW MolForm . CAS# Qual 1 2-Hexanoj<e 100 C6H12O 000591-78-6 91 2 2-HexaXone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 72 3 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 Propanal 58 C3H6O 000123-38-6 38 i\bundance Scan 150 (6.418 min): 25840.D (-) Wz 42795 100.00% 43

58 5000

100 6.00 6.20 a4o 'rct' aro m/z 58.05 62772% ■nfe-> 20 30 40 50 60 70 80 90 100110120130140 Abundance #1556:2-Hexanone 43

58 I .... I r.'r-f I I. . . I , . rryri* 5000 6.00 6.20 6.40 6.60 6.80 "raTz 417^5 18.80% 71 85 IM ■'M' 4- ,1, Tife-> ao'' 3o'' 40 '50' a 70 80 90 100 110 120 130 140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.00 6.20 6.40 6.60 6.80 ■ 5000 29 m/z SYTOO 14.90%

TiZz-> 20 ' 1' '' ' I • ■'. 11' ■ ■ I. 30 40 50 J, .7... ..... T............ 60 »1 «' • • 1 * ' ’ ' I ' ’ ‘ • I ‘ 70 80 90 100 110 ’ I * ' ' • I • • ‘ ’ I ' 120 130 140 140 Abundance #63354: Methyl Isobutyl Ketone 43 6.00' 6.^ " 6.40' ‘ 6,60 6.^ ‘ ra/FTooToo 12.24% 5000 58 85 100 67 •wy fa A Tlfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.oo' 'eio' 6.40 6.60 6.80

25840.D NP103001.M Wed Dec 05 15:33:12 2001 Page 1

NYC-WTC_000070163

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NYC-WTC_000070163Source: NYC Law Department, mirrored locally

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