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GCMS analysis results for sample AD24293, Nov 7 2001

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Laboratory report documenting GCMS analysis of sample AD24293 conducted on November 7, 2001, noting unknown compounds.

NYC-WTC_000068198–000068212

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068208
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NYC 9/11 Public Portal Document

Library Search Conipound Report Data File : C;\HPCHEM\1\DATA\OCT3101\24292 .D Vial: 11 Acq On : 1 Nov 2001 1:52 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DAT2kBASE\NBS75K.L Peak Number 3 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.66 0.53 ug/1 74127 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan( 102 C6H14O 000626-93-7 83 2 2-Pent, .ol, 4-methyl- 102 C6H14O 000108-11-2 78 3 2-Pe: rtanol, 3 -methyl - 102 C6H14O 000565-60-6 40 4 2- anol, (S)- 102 C6H14O 052019-78-0 40 <\bundance Scan 176 (6.662 min): 24292.D (-) ra/z 44.95 100.00% 4b

5000

41 69 6.40I 6.60 6.80 7.00 tT,Trm-.|l>..i 41 84^ -frrt+liliTj- 51 I? m/z i69.10 18.47%

L nZz-> 10 15 20% 30 35 40 45 50 55K)65 70 75 80 85 90 95 Abundance #63584:2-Hexanol 4|5

5000 A A 6.40 6.60 6.80 7.00 69 m/z 42.95 16.54%

TTfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90% .... I,............... Abundance #63545:2-Pentanol, 4-methyI- 4b 6.40 6.60 6.80 7.00 5000- m/z 41.05 16.08%

69 27 I''" I 3942 , 57 i n r, u 1111111111. ,,..,1...... TiZz-> 10 15 20 25 30 35 40 45 50 55 60 % 70 75 80 85 90 95 Abundance #1777:2-Pentanol, 3-methyl- 4b 6.40 6.60 6.80 7.00 m/z: 44.05 11.78% 5000

27 56 I'' “ H ‘ I ‘‘ ‘ I ‘ I'' I ‘‘ ‘ I " ‘' I ...... Sill.............................»4B7 I ‘ ‘ ‘ ’ I • ' ' ‘ I ' ' ' tVz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

24292.D NP103001.M Fri Nov 02 12:04:46 2001 Page 3

NYC-WTC_000068208

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NYC-WTC_000068208Source: NYC Law Department, mirrored locally

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