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GCMS analysis results for sample AD24293, Nov 7 2001

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Laboratory report documenting GCMS analysis of sample AD24293 conducted on November 7, 2001, noting unknown compounds.

NYC-WTC_000068198–000068212

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068209
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24292.D Vial: 11 Acq On : 1 Nov 2001 1:52 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.45 ug/1 201031 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 42 2 CH2=CHCH2p<0)OCH3 100 C5H8O2 003724-55-8 10 3 5-Hexenx^one 98 C6H10O 000109-49-9 9 4 3-Hydpdxy-2-pentanone___________ 102 C5H10O2 003142-66-3 9 Abundance Scan 288 (7.690 min): 24292.D (-) m/z 42.95 100.00% 40

59 5000 101 fp-p '7.^ 7.6o"7.^ 8,00 71 83 pT+q+rrrprrp m/z 59705 54.29% ■n&-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1(X) 105110 Abundance #64274:2-Pentanone, 4-hydroxy-4-tnethyl- 40

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 23.00% 27 101 83 l"ll.

L 49 .......I ttZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #1448: CH2=CHCH2C(O)OCH3 40 7.40 7.60 7.80 8.00 5000 m/z 58.05 16.82%

? 11.... I. I1, 11II,, I7 100 rrtTT T)fe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #1291:5-Hexen-2-one ... 43 7^ 7,60 7.80 8.00 m/z -41.00 8.10% 5000

nfe-> 55 pTTT^rtT-TTTpTTTpTT^TTTpTTTpT^^ L ' '7.46' '7.6O 7.M 's.oo' '

24292.D NP103001.M Fri Nov 02 12:04:49 2001 Page 4

NYC-WTC_OOO6682O9

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NYC-WTC_000068209Source: NYC Law Department, mirrored locally

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