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GCMS analysis results for sample AD24214, Nov 1 2001

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Laboratory report documenting GCMS analysis of sample AD24214 conducted on November 1, 2001, noting unknown compounds.

NYC-WTC_000067950–000067961

Folder label: “GCMS Scan X 10/9/01 An 10/31/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\24214.D Vial: 23 Acq On : 31 Oct 2001 1:23 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.62 ug/1 136105 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual. 1 2-Pentanone,hydroxy-4-methy1- 116 C6H12O2 000123-42-2 28 2 Acetone 58 C3H6O 000067-64-1 9 3 4-Hydro: 3-hexanone 116 C6H12O2 004984-85-4 9 4 5-Hexen. one 98 C6H10O 000109-49-9 7 Abundance Scan 289 (7.699 min): 24214.D (-) ra/z 42.95 100.00% 4)3

59 5000 101 71 .,•^..,■...1,1................ _Zz^_7S_7SI^8S__ ... nn/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000 59 7,40 7.60 7.80 8,00 m/z 100.95 20.59% 27 101 1. ■ , ,, ,1. ,1, , , , , I 83 " I " ■ ■ I ' )nfe-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #62322: Acetone 43 ... I.... I J , I,,,, 7.40 7.60 7.M 8.00 5000 m/z 58.05 18.48% 58 27 i-r-ryn nZz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #3241:4-Hydroxy-3-hexanone 50 7.40 7.60 7.80 8,00 31 m/z 40.95 7.13% 5000

I 45 87 116 ' I ' ' ‘ ‘ ' I ' I ' 70 ' M ' "go’'' ioo 110 IM nfe-> 20 30 40 50 60 '7.46' zm' zm' 's.bo'

24214.D NP103001.M Thu Nov 01 12:06:45 2001 Page 2

NYC-WTC_000067959

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NYC-WTC_000067959Source: NYC Law Department, mirrored locally

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