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GCMS analysis results for sample AD24214, Nov 1 2001

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Laboratory report documenting GCMS analysis of sample AD24214 conducted on November 1, 2001, noting unknown compounds.

NYC-WTC_000067950–000067961

Folder label: “GCMS Scan X 10/9/01 An 10/31/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\24214.D Vial: 23 Acq On : 31 Oct 2001 1:23 pm Operator: 209 GALOS Sairqole : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.54 ug/1 119396 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-DichlQa;febenzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-J/f2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Benzal ^yde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 Vanil^ n 152 C8H8O3 000121-33-5 9 Abundance z Scan 711 (11.573 min): 24214.D (-) m/z 149.90 100.00% 1$0

5000 115 52 78 -r-p-r-r-r-p-r * * I ’ 11.20 11.40 11.60 11.80 12.00 40 ■ I "’''I' 66 i 4U- m/z 151.90 64.78% Tlfe~> 30 40 50 60 70 80 90 iroi10 120 130 140 150 160 Abundance #9593:1.4-DichIorobenzene-d4 1!!0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 37.65% 35 I'''' I ' 30 " "40 ' M 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-<i4-, 5,6-<iichloro- 1!i0

115 11.20 11.40 11,60 11,80 12.00 5000 52 78 ra/z 78.05 20.02%

87 Tl/Z-> ' 35 I "40' " OT ‘ I'''' 1 ‘' I' 60 70 80 90 100 110 120 130 I A T 140 150 160 ^bundance #66892: Benzaldehyde. 2-hydroxy-3-methoxy- 152 11.20 11.40 11.60 11.80 12.(X) in/z 52.00 17.53% 106 5000- 53 81

92 122 ..136.......... 1 ' 1 ‘ ‘ ' I ' ' ’ * 1 * ‘ ‘ I * ' ' * 1 ' ’ ’ ‘ I ‘ -t+- ' I' ‘‘ 1''' • I TT-p 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1V20' '1140' it60 '11 .eo' ‘izoo

24214.D NP103001.M Thu Nov 01 12:06:47 2001 Page 3

NYC-WTC_000067960

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NYC-WTC_000067960Source: NYC Law Department, mirrored locally

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