GCMS analysis results for sample AD25459, Nov 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25458.D Vial: 5 Acq On : 16 Nov 2001 6:56 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.54 ug/1 89624 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tent^ive ID MW MolFoirm CAS# Qual

1 2-Pentanone, 4<-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 56 2 5-Hexen-2-Qjre 98 C6H10O 000109-49-9 9 3 Acetone 58 C3H6O 000067-64-1 9 4 1,3-Dio^ lane-2-methanol, 2,4-dimet 132 C6H12O3 053951-43-2 9 Abundance Scan 289 (7.699 min): 25458.D (-) m/z 42.9.5 100.00% 40

5000 59 101

83 7Ag 7;60 V80 8;00 51 TTpT4TTKTTyrrT-rp- M'Nipinl I....... . n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 40

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 :23.51% 27 83 101 I ■ ■ 1111"' I" " I ....... Ih|Iu.i.......I tt/2-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1291:5-Hexen-2-one 43

7.40 7.60 7.80 8.00 5000 m7z 58.05 ;18.59% 55 50 69 83 98 ... I" " I " 1111 Tife-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62326: Acetone 43 7.40 7.60 7.80 8.00 m/z 41.00 8.60%

5000 58

.................................................... TT/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 7.40 7.60 7.80 8.00

25458.D NP103001.M Wed Nov 21 11:56:50 2001 Page 1

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