GCMS comments for sample AD26478 showing no non-target compounds

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\26478.D Vial: 3 Acq On 7 Dec 2001 7:56 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 2-Butanol, 3-methyl-, (S)- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.16 12.54 ng/uL 3660750 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Butanol, 3-methyl-, (S) - 88 C5H12O 001517-66-4 42 2 1,2- Propanediol , 3 -methoxy- 106 C4H10O3 000623-39-2 36 3 2,3 -Butanediol 90 C4H10O2 000513-85-9 33 4 2-Butanol, 3-methyl- ______ 88 C5H12O 000598-75-4 9 Abundance Scan 253 (7.159 min): 26478.D (-) m/z 45.10 100.00% 45 5000 61 73 ' ■ i 1 1 1 • I ' • 6.80 7.00 7.20 7.40 7.60 36 41, | ,| 56 ।, ,, 78 88 m/ z 43.0.5 63.98% miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #852:2-Butanol, 3-methyl-, (S) 45

5000 ■ ‘ । i ■ » » । । TImTT 6.80 7.00 7.20 7.40 7.60 m/z 61.10 35.83% 27 39 । 55 73 87 ommmmptmmmmmmm m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63660: 1,2-Propanediol, 3-methoxy- 45

6.80 7.00 7.20 7.40 7.60 5000 75 rn/z 73.05 3 5.47% 31 61 15 88 TTDLTmmmmugp TH m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #917: 2.3-Butenediol 45 6.80 7.00 7.20 7.40 7.60 ‘ I ' 1 ■ 1 i 1 1 ‘ 1 i 1

m/ z 44.0.5 12.81% 5000

29 .. 19.. LL... , I ,.. 7.... 75 ...9Q... TTTTEmTrrg miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.80 7.00 7.20 7.40 7.60

26478.D NP112701.M Thu Dec 13 11:22:23 2001 Page 9

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