GCMS comments for sample AD26478 showing no non-target compounds

NYC 9/11 Public Portal Document

Library Search Compound Report 2 Data File C:\HPCHEM\l\DATA\DEC0701\26478.D Vial: 3 Acq On 7 Dec 2001 7:56 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1-Butene, 2,3-dimethyl- Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

7.51 0.42 ng/uL 122112 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butene, 2,3-dimethyl- 84 C6H12 000563-78-0 37 2 1-Butene, 2,3-dimethyl- 84 C6H12 000563-78-0 25 3 2-Pentene, 4-methyl-, (E) - 84 C6H12 000674-76-0 25 4 2-Pentene, 2-methyl - 84 C6H12 000625-27-4 25 Abundance Scan 291 (7.507 min): 26478.D (-) m/z 41.10 100. .00% 4i 69 5000

' TITTrTTT ■“ i • ■ ■ ' i

7.20 7.40 7.60 7.80 38 45 49 53 58 Tmmmmmmm 84 m/z 69.10 63.87% m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62760: 1-Butene, 2,3-dimethyl- 41 69

5000 -*418 ‘A1-F*1111‘11111‘T 7.20 7.40 7.60 7.80 27 84 m/ z 43.00 47, .32% 15 51 55 ■ ■111 ■ —mmmmmmmmm

T m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #590:1-Butene, 2,3-dimethyl- 41 69 1i 1 1 1It I | I IT I | I 1 TTI 7.20 7.40 7.60 7.80 5000 m/z 39.10

27 84 ‘ 1’11119121111111 37 , 51 55 111'11"" I'11' 111" 1111' 1111' 111" 11" | . “ •! • ' ■ ‘ | | | . miz-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 #62774: 2-Pentene, 4-methyl-, (E)- 41 7.20 A..L 7.40 7.60 7.80 1T

m/z 71.0,5 23.97% 69 5000

27 84

miz—> 5 — mmmmH 3 ’ 1—00101111 55 —P l — 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 i ’11' i p-rrrp-rr A • • 11 11 T I • 7.20 7.40 7.60 7.80

26478.D NP112701.M Thu Dec 13 11:22:26 2001 Page 10

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