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GCMS results log, sample AD26982, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26982 completed on December 11, 2001, noting unknown compounds.

NYC-WTC_000032343–000032361

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0601\26982.D Vial: 24 Acq On 7 Dec 2001 7:05 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Butanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.18 2.25 ng/uL 932184 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, methyl- 88 C5H120 000598-75-4 9 2 2,3-Butanediol 90 C4H10O2 000513-85-9 9 3 Propane, 2-ethoxy- 88 C5H120 000625-54-7 9 4 1,2-Propanediol , 3-methoxy­ 106 C4H10O3 _______ 000623-39-2 9 Abundance - Scan 255 (7.183 min): 26982.D (-) m/z 45.05 100.00% 45

5000 6.1 73

6.80 7.00 7.20 7.40 7.60 i"' 'i i"" r IHm 88 TI TTC"ung r'" i1 207 m/ Z 43.00 84.25% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62961: 2-Butanol, 3-methyl- 45

5000 6.80 7.00 7.20 7.40 7.60 73 m/ z 61.00 34.70% 55

m/z-> TIT 27 TTTTT LX i" ■11 ■"11 TTTTT 87— r r" ■ r'" i" " r r " T" "IFTTTTTTTTTTTTTT 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #917: 2,3-Butanediol 4.5 6.80 7.00 7.20 7.40 7.60 5000- m/z 73.0,5 32.43% 29 19 57 75 90 TTCCu"uu"I"nt —"u0—un"tuu—EU—"10"91"1"TT "i•■■•। ■i■ m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62955: Propane, 2-ethoxy- A.......... — 45 6.80 7.00 7.20 7.40 7.60 m/z 44.00 19.64% 5000- 73 27 59 88 ........................ --===== i‘ ■i MH | 'k*1|।।| । | । |।|।| m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 6.80 7.00 7.20 7.40 7.60

26982 .D NP112701.M Tue Dec 11 14:48:51 2001 Page 5

NYC-WTC_000032355

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NYC-WTC_000032355Source: NYC Law Department, mirrored locally

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