GCMS comments for sample AD26478 showing no non-target compounds

NYC 9/11 Public Portal Document

Library Search Compound Report $ Data File C:\HPCHEM\1\DATA\DEC0 701\26478.D Vial: 3 Acq On 7 Dec 2001 7:56 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS 'Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 2-Pentene, 4-methyl-, (Z)- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

6.71 0.54 ng/uL 158466 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentene, 4-methyl-, (Z)- 84 C6H12 000691-38-3 28 2 1-Hexene,3, 3-dimethyl- 112 C8H16 003404-77-1 10 3 2-Butenal, (E) - 70 C4H60 000123-73-9 9 4 2-Butenoic acid, 4-nitrophenyl este 207 C10H9NO4 014617-88-0 9 Abundance Scan 204 (6.709 mln): 26478.D (-) "I" ■m/z

L 69.10 100.00% 41 69

5000

53 ‘11/8/8 TWPA TT . III 58 . 84 6.40 6.60 6.80 7.00 11 1-------- ■ • i • • ■ • i ■ ■ ■ • i • ‘ ‘ 1 1‘ ‘ 1 1 1 ‘ ‘ m/z 41.05 97.61% miz-? 10 20 30 40 50 60 70 80 90 100 110 Abundance #62772: 2-Pentene, 4-methyl-, (Z)-

5000 41 69

WAK/A TmmTTTT 6.40 6.60 6.80 7.00 84 27 m/z 43.10 86.50% 53 115..... 1 , TI - l —PIT ' ‘ I ' ' ' ' I ' 1 1 1 I ' 1 ■ i ■ ‘ ■ ■ I ' 1 1 1 I ' 1 1 1 I miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64048: 1-Hexene. 3.3-dimethyl- 41

69 11 ■ i ■ 6.40 6.60 -PP 6.80 7.00 55 5000 m/z 71.00 61.99%

miz-> Abundance * * i ' * * * । * 1 1 * । '' • * । * *1 * r*• * * i * 1 * • ।1'* *।'* * 1।*1 *'i* 11 11 * 1 *1 i 10 20

27 30 40 41 50 60 70 #62443:2-Butenal, (E) 70 83 80 97 90 112 100 110 LN.. m/z 6.40 6.60 70.05 6.80 7.00 20.41% 5000

33 11 ■ • 1148,55 ..... | HL • ■ i ' • ■ ■ i ■ ■ ' • i 1 1 1 1 I ' 1 1 1 I ------- A- m/z~> 10 20 30 40 50 60 70 80 90 100 110 6.40 6.60 6.80 7.00

26478.D NP112701.M Thu Dec 13 11:22:20 2001 Page 8

NYC-WTC_000031754