GCMS analysis result with unknowns, Dec 2001

NYC 9/11 Public Portal Document

Library Search. Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26391.D Vial: 7 ' Acq On : 30 Nov 2001 5:41 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexene-2,5-diol Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.03 1.00 ng/uL 468895 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexene-2 /5-diol 116 C6H1202 007319-23-5 38 2 4-Penten-2 -one, 4-methyl- 98 C6H10O 003744-02-3 36 3 3,5-Hex; dien-2-ol 98 C6H10O 003280-51-1 28 4 1-Butan 1, 2-ethyl- 102 C6H140 000097-95-0 17 Abundance 7. Scan 21 (5.032 min): 26391 .D (-) m/z 43.00 100.00% 43

5000

39 1 51 55

70 94 | 83 98 _/W —! l l . > I M . | I I ■ . | I . . . ( 4.90 5.00 5.10 5.20 5.30 5.40 . I . . . 4 | .

"I"' mmT —H mHH 1puntu——gmmy- m/z 83.05 30.85% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #3285: 3-Hexene-2,5-diol 43

5000 —Im 4.90 5.00 5.10 5.20 5.30 5.40 55 83 m/z 30.72% 98 . 61 71 TmHpp . ।. > > > t.. ।। > 11. । >. > < ।< mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1244: 4-Penten-2-one, 4-methyl- 43 CAAA meATAR 4.90 5.00 5.10 5.20 5.30 5.40 5000 m/z 41.00 18.85% 83 29 39 55 98 TpTHHHmmmp mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1271: 3,5-Hexadien-2-ol 43 4.90 5.00 5.10 5.20 5.30 5.40 7 m/z 42.00 16.50% 5000 55 83 79 98 51 71 , 1’1’1221117 ’I 1111111133 — TTTH - TIeaug i' • • • t • m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40

26391.D NP112701.M Tue Dec 04 10:42:25 2001 Page 1

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