GCMS analysis results for sample AD26624, Dec 10 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26624.D Vial: 7 Acq On 6 Dec 2001 3:39 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Butanol, 3-methyl-, (S)- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.20 7.42 ng/uL 1729600 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3-methyl-, (S) - 88 C5H12O 001517-66-4 42 2 1,2-Propanediol, 3-methoxy- 106 C4H10O3 000623-39-2 36 3 2,3-Butanediol 90 C4H10O2 000513-85-9 33 4 N-Ethyl formamide 73 C3H7NO _______ 000627-45-2 9 Abundance Scan 257 (7.201 min): 26624.D (-) m/ z 45.0,5 100.00% 45

5000 61 73 I | — I I | I T < / | 17-

6.80 7.00 7.20 7.40 7.60

m/z—> 0- 5 401 +56 1P— i ■ " ■ i" ■ ■ i 1 . . TTT 84 88 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/ z 4 3.00 66.55% Abundance #852: 2-Butanol. 3-methyl-, (S)- i 45

5000 = -PP-PT P -PPP 6.80 7.00 7.20 7.40 7.60 m/z 73.0,5 35.15%

m/z-> 5 i ■■ ■ ■ i 27 — 39 | 55 73 m 87 TTTTT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 'Abundance #63660: 1 2-Propanediol, 3-methoxy- 4'5

6.80 7.00 7.20 7.40 7.60 5000 75 m/z 61.10 33.73% 31 61 15 I i 88 i l I * * ” 111" I'1 • • I I‘ ‘I ■p-rrr 1 ’ " 11 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #917: 2,3-Butanediol - 45 6.80 7.00 7.20 7.40 7.60 m/Z 44.00 14.38% 5000

29 57 m/z-> t 19 mH | ,........., | 75 90 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 " " i ■" ■ r'" i" " r TTTTTTT 1111 < 111111111111111 (111111 > -------- 6.80 .J 7.00 7.20 7.40 7.60

26624.D NP112701.M Fri Dec 07 14:47:46 2001 Page 2

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