GCMS results log, sample AD26983, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26983.D Vial: 25 Acq On 7 Dec 2001 7:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Tetrahydrofurfuryl chloride Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.14 0.53 ng/uL .191338 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetrahydrofurfuryl chloride 120 C5H9C10 003003-84-7 50 2 2-Hepten-3-gX 4,5-dimethyl- 142 C9H180 055956-37-1 38 3 Cyclopentanol, 1-methyl- 100 C6H120 001462-03-9 36 4 Cyclopentanol , l-methyl- 100 C6H120 001462-03-9 28 Abundance Scan 141 (6.138 min): 26983.D (-) m/z 71.05 100.00%| 71

5000 43 ........ A tr r . . . . । . . . . । . ,-r . j . . 1111

miz-> 10 20 30 J— IL.... L 40 50 60 57

701 80 H I | | i . , - .1.1

90 100 • ■ r, | I i b | | | | i , p-

100 110 120 130 5.80 6.00 6.20 6.40 m/z 43.10 44.70% Abundance #3704: Tetrahydrofurfuryl chloride 71

5000 43 ... AN 5.80 6.00 6.20 6.40 m/z 41.10 27.39%

M 27 49 55 62 77....................................... । , i 120 ■ ' i ' 1 TTT m/z-> 10 20 30 40 50 60 701 80 90 100 110 120 130 Abundance #8051: 2-Hepten-3-ol. 4,5-dimethyl- 7.1

5.80 6.00 6.20 6.40 5000 43 m/ z 42.1,0 21.38% 27 15 55 i 124 81 100 109 i ‘ETEETEIETTLI‘‘111EEEET"T--IEET11111*_*EECT"ITI ‘I-TEICTTrrT ‘T- m/z-> Abundance 10 20 30 40 50 60' 70 80 90 #1511: Cyclopentanol, 1-methyl- 100 110 120 130

71 MA —A4 5.80 6.00 6.20 6.40

43 m/ z 3 9.0,0 11.26% 5000 58

85 i 15 27 | ■ ■ i ■ ■ ■'I 1111 I 111 1 I..... . 11 1 i ■ ■ ' 1 i1 — , 100 r1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.80 6.00 6.20 6.40

26983.D NP112701.M Tue Dec 11 14:49:39 2001 Page 4

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