GCMS analysis result with unknowns, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26391.D vial: 7 Acq On : 30 NOV 2001 5:41 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Hexanol Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 6.72 0.53 ng/uL 247663 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance Scan 205 (6,719 min): 26391.D (-) m/z 59.10 100.00% 59

5000 73 43 6.40 6.60 6.80 7.00 m Hm 53+ - 4 tmpt . ।. b . ■ |.. 11141 1. 111.11 1.11 j.. 111.1.. j 1 m/z tt t 55.10 77.04% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528: 3-Hexanol 59

73 5000 * * » , • * » * । » * > > । * PMTffT 31 6.40 6.60 6.80 7.00 m/z 73.05 43.34% 45 ■ * । •1 • • i ■1 * ■ । mH +4 tmm "—uuu84 —ut———"unpir miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #63529:3-Hexanol 59 6.40 6.60 6.80 7.00 5000 31 73 m/z 43.05 27.02%

44 miz-> .....+.. — +1 tpp ’ 1’11117 11 102 I’ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 j. . 1 . |b i, i,..., । . .. , ( 11 ■ ■11

Abundance #63531:3-Hexanol bipiii TITTTr t > i • i r. । 59 6.40 6.60 6.80 7.00 m/z 41.00 24.93%

Uy, 5000- 73

miz—> 43

nUUTp-rrT +4 tpp 11... 11.. b. 11 b.. ।.. 111. b b. ।... b 11.. 11. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 110 U • ■ । 6.40 k । ■ ■ • ■ । ■ • ■ • । 6.60 6.80 7.00 ■ i

26391.D NP112701.M Tue Dec 04 10:42:28 2001 Page 7

NYC-WTC_000031523