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GCMS analysis result with unknowns, Dec 2001

Machine-extracted title · confidence 100%

Analysis report for sample AD26391 indicating the presence of other unknown compounds on December 4, 2001.

NYC-WTC_000031509–000031529

Folder label: “GCMS X 11/5/01 A 12/1/01

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Scanned page image, NYC-WTC_000031522
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26391.D Vial: 7 Acq On : 30 Nov 2001 5:41 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise t Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Hexanone Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 6.59 0.47 ng/uL 220983 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2 -Hexanone 100 C6H120 000591-78-6 90 2 2-Hexanone 100 C6H120 000591-78-6 90 3 2-Hexanone 100 C6H120 000591-78-6 90 4 2-Hexanone 100 C6H120 000591-78-6 86 Abundance Scan 191 (6.591 min): 26391 .D (-) m/z 43.00 100.00% 43 58 5000 J■—। । । । । । । । । । । । i > । > । । । > । । > i 6.20 6.40 6.60 6.80 7.00 1. 50 1 71 85 100 miz-> m-mmmmmmmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/z 58.10 53.86% Abundance #63386:2-Hexanone 43

5000 58 - T14. — TAT 6.20 6.40 6.60 6.80 7.00 29 m/z 57.05 14.53% ! 71 85 mpanmmmmmmmmmm100 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385:2-Hexanone 43

6.20 6.40 6.60 6.80 7.00 5000 58 m/z 41.05 13.84% 29 । | 71 85 100 mmmmm m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384:2-Hexanone j 43 6.20 6.40 6.60 6.80 7.00 m/z 100.05 9.69%

5000 58 29 t j 11 > i! < 11 > ] ■ 1 + 71 85 100 m/z—> TPIT m TOmp] 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

26391.D NP112701.M Tue Dec 04 10:42:28 2001 Page 6

NYC-WTC_000031522

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NYC-WTC_000031522Source: NYC Law Department, mirrored locally

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