NYC-WTC_000031350
Calibration data table for gas chromatography-mass spectrometry analysis dated December 3, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS calibration table for TCLP analysis, Dec 2001
Machine-extracted title · confidence 100%Calibration table listing standards like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 for GC/MS analysis dated December 2001.
NYC-WTC_000031876–000031888Folder label: “GCMS X 11/7/01 A 12/6/01”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC0 6 01\LBA.D Vial: 10 Acq On 6 Dec 2001 6:23 pm Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Hexanol Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
6.72 0.62 ng/uL 158984 1,4-Dichlorobenzene-d4 11.89
Hit# of 5 'entative ID MW MolForm CAS# Qual
1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 72 3 3-Hexanol 102 C6H140 000623-37-0 64 4 3-Hexanol Abundance Scan 205 (6.719 min): LBA.D (-) 102 C6H140 000623-37-0 56 m/z 59.10 100.00% 55 59
5000 73
41 • • । 1 ■ ■ ■ । 6.40 6.60 6.80 7.00 1 45 TIIPmmp 84 4 tpp TITLg m/z 55. 0 77.25% miz-? 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol - ...... ” 59 55
5000 31 73 YIAA —M 27 6.40 6.60 6.80 7.00 m/ z 73.05 43.94% 44 " i" ■ ■ । mmdmm ___________________ 102 ppmpH 11211’0010301100—1017’ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531:3-Hexanel 59 55 ' ■ ' i ■ ■ ■ ■ i ■ ' ■ ■ i ■ ■ 1 ■ i ■ ■ 1 r i
6.40 6.60 6.80 7.00 5000 73 m/z 41.05 19.04% 43
m/z-> Abundance •........... 39 ....... _ 69 _________________ 1’’!1""191111120091110100100101002000T—0/00010010020000upg 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #1762:3-Hexanol
55 59 m/z 6.40 AANJ 6.60 43.00 6.80 7.00 16.69% 31 5000 27 43 73
. > I I , , , I . . , q < II I [I I| | | | | | , , , , | ।I [I |I I |। | I ■ | | | , | ! | , ।I I | | I | I , | , I , ! | ! U I | , I I I | , , , , I102 .... I . . . . | . I— , , , , I , , ,, |, 1 1 1 I ' TTTTr Ti • TT • TT I । । । r j m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 6.40 6.60 6.80 7.00
LBA.D NP112701.M Wed Dec 19 13:08:48 2001 Page 2
NYC-WTC_000031883
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NYC-WTC_000031883Source: NYC Law Department, mirrored locally
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NYC-WTC_000031814
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 3.4 ug/L in sample AD2653S.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032269
Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 6, 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031831
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 3.2 ug/L in sample AD26536.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031665
Instrument output file listing calibration standards and response factors for various compounds used in the December 7, 2001 analysis.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031415
Report documenting GCMS analysis of sample AD26386 with a note regarding unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031213
Data table containing pH and volume measurements associated with GCMS method 208 analysis procedures.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031433
Report documenting GCMS analysis of sample AD26387 with a note regarding unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031775
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 0.72 ug/L in sample AD26533.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031762
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 0.80 ug/L in sample AD26532.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031739
Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26478 revealed no non-target compounds.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031550
DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26393 noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Filed elsewhere
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NYC-WTC_000031869
Illegible text on a single page from the GCMS folder covering November to December 2001.
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NYC-WTC_000031870
Index or cover sheet page for the GCMS folder covering the period from November 7 to December 6, 2001.
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NYC-WTC_000031889
GC/MS analysis of sample AD26538 identified other unknown compounds noted in comments section, December 10, 2001.
Filed in the same folder
NYC-WTC_000031905
Laboratory report documenting GCMS analysis of sample AD26624 identifying unknown compounds on December 10, 2001.
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NYC-WTC_000031920
Laboratory report documenting GCMS analysis of sample AD26625 identifying unknown compounds on December 10, 2001.
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