GCMS calibration table for TCLP analysis, Dec 6 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 10 2-Hexanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

10.53 0.54 ng/uL 199001 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

l 2-Hexa: 1 102 C6H140 000626-93-7 64 2 2-He Anol 102 C6H140 000626-93-7 59 3 2-Hi xxanol 102 C6H140 000626-93-7 50 4 2-1 entanol, 4-methyl- 102 C6H140 000108-11-2 50 Abundance Scan 620 (10.529 min): LBB.D (-) m/ z 43.10 100.00% 43 __ 5000 J \ 57 85 ' 1 1 ’ * "11 69 10.20 10.40 10.60 10.80 —H TTr rl —................ ............. m/z 45.10 83.22% m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63582:2-Hexanol : 45

5000 I ‘m 10.20 10.40 10.60 10.80 27 69 m/z 41.10 29.97% 19 ! 57 I 87 111111 " I " " TTT • I • " ’ I Ti Tit r " • r ■" r • ■ ■ i r'" । 1111111111111111 m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1792; 2-Hexanol i 45 —M I' ' 1 1 1 ' ' 1444*, 10.20 10.40 10.60 10.80 5000- m/z 85.05 17.81%

27 39 55 69 87 T i11111 111" l111 11' ’' I" " 111' ‘ I •' ‘' I Trrr T'1 " ।' I m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63583: 2-Hexanol 45 10.20 10.40 10.60 10.80 m/z ,57.10 17.43% 5000

1

I • • “ Iu " I 473R.+ m/z->10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 — 55 69 । 87 .।| i 11. ।।11.... ।. TTT ri 111111 ■ 111111111111111111111 I I 10.20 A 10.40 10.60 10.80

LBB.D NP112701.M Wed Dec 12 08:19:17 2001 Page 10

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