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GCMS Analysis Report for Sample AD26387, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26387 with a note regarding unknown compounds.

NYC-WTC_000031433–000031451

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Coirpound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26387.D vial: 13 Acq On : 30 Nov 2001 11:08 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Butanol, 3-methyl-, (S)- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.19 7.16 ng/uL 3464860 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3-methyl-, (S) - 88 C5H120 001517-66-4 38 2 2-Butanol,3-methyl- 88 C5H120 000598-75-4 9 3 Butane, -ethoxy- 102 C6H140 002679-87-0 9 4 Ethanol 2-methoxy-, carbonate (2:1 178 C7H14O5 000626-84-6 9 Abundance Scan 257 (7.195 min): 26387.D (-) m/z 45.00 100.00% 45

5000 73 61 . । . 1 . . । l ■. .- . ! r i . , । , i . i । . . 6.80 7.00 7.20 7.40 7.60 mll 91__________________________________ 207 l.. । ... 11'.... ।.... ।.... ।.... ।.... ।.... । .... ।.. .. (.... ।.... । .... ।.... , m/z 43.0.0 54.27% m/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #852:2-ButanoI, 3-methyl-, (S)- 45

5000 TTTETTiPPPamT 11 • * 6.80 7.00 7.20 7.40 7.60 m/z 73.0.5 41.14% 55 73 ... .......... ’1’’11771 87................................................. Jl. 11111111110111111111111710109119110111111100100111001000010111507 miz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62962: 2-Butanol, 3-methyl- 45

6.80 7.00 7.20 7.40 7.60 5000 m/z 61.00 38.05%

27 55 73 ........................... 1..... 8?................................................................ 1 11 ‘' "I*' ‘* 11 131101113 | " " I •. ■. I |.... |.. ■. 111111 n i r| iTnp-r ri 111111111111 H 1111111 > 11 mz-> :20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #63540: Butane, 2-ethoxy- 1 i ■ ■ ■ 1 i ‘ 45 6.80 7.00 7.20 7.40 7.60 m/z 44.0.5 10.88% 73 5000

27 59 _ . — ir

m/z—> — + 87102....................................... 11 •1 *' i'1 “ i" ■ ‘ i “1 ■ i1" ■ i “ " i ■11 ■ i1"111 ■111 “ “ i1111111" i1111 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 6.80 7.00 7.20 7.40 7.60

26387.D NP112701.M Tue Dec 04 10:39:15 2001 Page 6

NYC-WTC_000031446

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NYC-WTC_000031446Source: NYC Law Department, mirrored locally

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