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GCMS Analysis Report for Sample AD26336, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26336 with a note regarding unknown compounds.

NYC-WTC_000031384–000031399

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26336.D Vial: 30 Acq On : 1 Dec 2001 2:36 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Butanol, 3-methyl-, (S)- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.17 2.08 ng/uL 666837 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Butanol, /3-methyl-, (S) - 88 C5H120 001517-66-4 40 2 2-Butanol/ 3-methyl- 88 C5H120 000598-75-4 40 3 Isopropyl Alcohol 60 C3H80 000067-63-0 37 4 1,2-Propanediol, 3-methoxy-______ 106 C4H10O3 000623-39-2 36 Abundance 7 Scan 254 (7.168 min): 26336.D (-) m/z 45.10 100.00% 45

5000 61 73 : i | ill i | i I । 1 j it i t । । i T i । i 6.80 7.00 7.20 7.40 7.60 miz-> mHHm 1 ' i' ■" i‘ ■" i 88 207 ■.11... j. >..j.... ।. j....t.... ।...., 20 30 40 50 BQ 70 80 SO 100 110 120 130 140 150 160 170 180 190 200 210 , p-rrTyrrTTp-m-p m/z 43.00 66.13% Abundance #852:2-Butanol, 3-methyl-, (S)- 45

5000 BiB. TT TT[I8T । I i i l i | t t U I | :

680 7.00 7.20 7.40 7.60 m/z 61.00 35.62% 27 , 55 73

mlz-> 4 7 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 20 30 Abundance #62961: 2-Butanol, 3-methyl- 45 i i । । i i I F UI II J I J 1 1 1 1 | U) 6.80 7.00 7.20 7.40 7.60 5000 m/z 73.05 35.18%

55 73 27 mH —.,. m.1 Tmm 87 mlz-> 20 30 40 50 60 70 80 90 1001) 120130140150160170180190 200 210 Abundance #62359: Isopropyl Alcohol 45 6 80 7.00 7.20 7.40 7.60 m/z 44.05 13.67% 5000

27 I.It IIit, 59 t _______________________________ tW । j i»11’t 1111111111111M1111 n j 11111111:111111111111111111 i 11111111111 j 111 r pi 11111 h 11111 i : | I • I i | i I i I | I I T I J T I T T IB m/z—> 2030405060 70 8090 100110120130140150160170180190200213 6.80 7.00 7.20 7.40 7.60

26336.D NP112701.M Tue Dec 04 15:07:51 2001 Page 4

NYC-WTC_000031395

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NYC-WTC_000031395Source: NYC Law Department, mirrored locally

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