GCMS calibration table for TCLP analysis, Dec 5 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0501\26712.D Vial: 3 Acq On 5 Dec 2001 10:35 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Propanone, 1-cyclopropyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

5.01 1.58 ng/uL 552784 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone/ 1-cyclopropyl- 98 C6H10O 004160-75-2 9 2 Heptane, 2,3-dimethyl- 128 C9H20 003074-71-3 9 3 2-Pentane ne, 3-methylene- 98 C6H10O 004359-77-7 7 4 5-Hexen— -one 98 C6H10O 000109-49-9 7 Abundance Scan 18 (5.010 min): 26712.D (-) m/z 43.00 100.00% 1 43

5000-

......... . 55 69 T 98 ' I ' ' ' ’ I ' ' ' • I ’ ' ' ' I 1 +1T111 t.... 11,.. ।।. 111।।।।. 4.90 5.00 5.10 5.20 5.30 5.40 m/ z 83.05 13.73% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1306: 2-Propanone, 1-cyclopropyl- 43 _ / 5000 i 11' ' I i ' 1 ' ■ I 4.90 5.00 5.10 5.20 5.30 5.40 55 m/z 55.10 12.68% ! 29 1 m/z-> 10 20 II 30 11 ‘It 40 50 469 60 70 80 3-9 90 100 110 120 130 Abundance #5152: Heptane. 2,3-dimethyl- 43 TTTPT fr 4.90 5.00 5.10 5.20 5.30 5.40 — 5000 m/z 42.05 11.63% 57 84 27 71 , TT-p I_______________ • i ■ ■ • • i > • ■ ■ i > ‘ । • i > .... II........... 128 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 'Abundance #63190: 2-Pentanone, 3-methylene- T‘‘CIOUIC‘TCTU-TTTEIIITTT7r‘r‘1 43 55 4.90 5.00 5.10 5.20 5.30 5.40____

3 m/z 8.55% 5000 83 27 15 98 _....... | ■ ■ ।■ • ■ ■ । ■ TIT । • 37—4 - I।।1'1 । । 1 1 1 ■ I 'i ' 1।। TTTrT I 1 1 i ‘ ' i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 4.90 5.00 5.10 5.20 5.30 5.40

26712.D NP112701.M Fri Dec 07 13:15:07 2001 Page 1

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