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GCMS Analysis Report for Sample AD26388, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File | C:\HPCHEM\1\DATA\NOV3001\26388.D vial: 14 Acq On : 1 Dec 2001 12:02 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Oxirane, 3-ethyl-2,2-dimethyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.18 3.99 ng/uL 1753570 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 3-ethyl-2,2-dimethyl- 100 C6H120 001192-22-9 38 2 Pentane, 2,3-dimethyl- 100 C7H16 000565-59-3 35 3 Furan, tetrahydro-2, 5-dimethyl- 100 C6H120 001003-38-9 27 4 Oxirane, tetramethyl-_____________ 100 C6H120 005076-20-0 27 Abundance Scan 37 (5.185 min): 26388.D (-) m/z 41.05 100.00% 41 56

5000 71 5—r * 1 1 i 1 ■ 5.00 5.20 5.40i 5.60 ------- +’ I T 1 47 85 | 1-— 190— — m/z 56.10 74.81% miz-> 10 20 30 40 50 60 70 80 190 100 110 Abundance #1516: Oxirane, 3-ethyl-2,2-dimethyl- 59 41

5000 31 -T1 5.00 5.20 5.40i 5.60 85 m/z 59.10 74.37% 71 100 - ■ ' i ' ‘ 1 1 I 1T TT 40— ' 50 ' TITT । i । i ■ 1 1 1 I 1 1 1 1 i 1 mz-> 10 20 30 60 70 80 90 100 110 Abundance #63429: Pentane, 2,3-dimethyl- 43 55 ----- —P 5.00 5.20 5.40 5.60 5000 29 m/z 43.05 72.69% 71

15 85 100 -- ------- T-r-p-r 1 i1' '11 ri 1 11 * 1 •rr1 1 * i' 1 ■ 1 i * mlz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63368: Furan, tetrahydro-2,5-dimethyl- 41 55 5.00 5.20 5.40 15.60 m/z 42.10 62.87%

5000

tnfz~> — ———TI i'' ' I 1’ 10 20 27

30 40 50 67

TDmTTTBTT 60 70 80 90 100 110 85 100 5.00 L5.20 5.40 1 • I 1 5.60

26388.D NP112701.M Tue Dec 04 10:40:21 2001 Page 3

NYC-WTC_000031460

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NYC-WTC_000031460Source: NYC Law Department, mirrored locally

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