Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
NYC-WTC_000087447–000087457Folder label: “GC/MS Scan 9/19/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT0101\LBF.D Vial: 6 Acq On 1 Oct 2001 6:37 pm Operator: 209 GALOS Sample 9/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.49 ug/1 66477 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Hexanone 100 C6H12O 000589-38-8 83 2 Butan^< 2,2-dimethyl- 86 C6H14 000075-83-2 42 3 PentXne, 2,3,4-trimethyl- 114 C8H18 000565-75-3 40 4 Pqhrane, 3,3-dimethyl-__________ 100 C7H16 000562-49-2 38 \bunda&e Scan 146 (6.383 min); LBF.D (-) m/z 43705 100700% 43 57
71 5000 100
_6W__S__6^§_j60_^^ +T-' ' I II ' ' ' I ' 1'1 ' I I m/z 5776^0 8^717% 10 20 30 40 50 6070 80 90 100 110 120 Abundance #1528; 3-Hexanone 43 57
29 71 5000 ' I ' ' ' ' I ' ' ' ' I ' ' ‘ ' I ' ' 6.00 6.20 6.40 6.60 6.80 100 m/z 71(00 57.37%
.................... .... n4 Ur. ■....ll....... ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 ®ibundance #732; Butane, 2,2-dimethyl- 40 5(7 71 6.00 6.20 6.40 6.60 6.80 29 m/z 100.05 35767% 5000
■n/z-> Abundance 10 15 I 20 30 40
43 ' ' 50 ' 60 i'i 70
71 80 #64229; Penlane, 2,3,4-trimethyl- 90 100 110 120 LjrX. 6.00 m/z 6.20 41.05 4 6.40 6.60 21.19% 6.80
5000
uu 27 55 ■■•....n-J.,....... 'I I I I ' I ' ' ■ I I ' ' I I I ' 114 ni/z-> 10 20 30 40 50 60 70 80 90 100 110 120 6.00 6.20 6.40 6.60 6.80
LBF.D NP091101.M Wed Oct 03 14:32:40 2001 Page 1
NYC-WTC_000087453
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NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000087156
Gas chromatography-mass spectrometry scan results recorded on September 19, 2001 for environmental samples.
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Laboratory report detailing GC/MS analysis of sample vial 6 conducted on October 1, 2001, including method parameters and peak data.
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NYC-WTC_000087160
Laboratory report detailing GC/MS analysis of sample vial 6 conducted on October 1, 2001, including method parameters and peak data.
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NYC-WTC_000087163
Laboratory report documenting GC/MS analysis of sample AD22578 conducted on October 10-11, 2001, identifying unknown compounds.
Filed in the same folder
NYC-WTC_000087180
Laboratory report documenting GC/MS analysis of sample AD22579 conducted on October 11, 2001, identifying unknown compounds.
Filed in the same folder