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GC/MS calibration table for TCLP method, Oct 2001

Machine-extracted title · confidence 100%

Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.

NYC-WTC_000087132–000087155

Folder label: “508 Scan 9/18/01 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample : 9/18 Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************5)f************

Peak Number 1 3-Hexanone Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 6.38 1.07 ug/1 150086 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-He3c^one 100 C6H12O 000589-38-8 78 2 3-Pentanone, 2-methyl- 100 C6H12O 000565-69-5 53 3 Burane, 2,2-dimethyl- 86 C6H14 000075-83-2 45 4 2/4-Pentanedione 100 C5H8O2 000123-54-6 38 <\bund<fnce Scan 146 (6.384 min); LBE.D (-) m/z 43.00 100.00% 43 57

5000 71

100

P 6,00 m/z 6.20 57700 w 6.40 6.60 89.94% 6.80

n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1528; 3-Hexanone 57

29 71 5000 6.00 6.20 6,40 6.60 6.80 100 m/z 71.00 60.08% " " I" " I" " I'"' 111' ............. ..... ........ +TTTyTTTTp ................. I pfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63398; 3-Pentanone, 2-methyl- 5(7 43 6.00 6.20 6.40 6.60 6.80 5000 m/z 100.05 34.62% 100 71

Ti/z-> Abundance 5 I...... 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #732: Butane, 2,2-dimethyl- 43 5(7 71 85 .... I'

L 6.00 6.20 41.05 jyu 6.40 6.60 26.15% 6.80

29 5000

15 +TTpn^ P nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

LBE.D NP091101.M Wed Oct 03 14:40:57 2001 Page 1

NYC-WTC_000087138

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NYC-WTC_000087138Source: NYC Law Department, mirrored locally

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