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GC/MS analysis results for sample AD23797, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23797 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089446–000089460

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089454
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM \1\DATA\OCT3 OO1\23797.D Vial: 17 . Acq On : 31 Oct 2001 6:07 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 2 09 Mise Multiplr: 1.00. MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L **************************************** * * *******************'*****'^^A , Peak Number 1 3-Hexanone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.32 0.47 ug/1 69721 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 'Tentative ID MW MolForm CAS# Qual ■ 1 3 -Hexan^e 100 C6H12O 000589-38-8 91 2 3-Pent^one, 2-methyl- 100 C6H12O 000565-69-5 47 - 3 2,4-P^tanedione 100 C5H8O2 000123-54-6 43- 4 But^ e, 2,2-dimethyl-____________ 86 C6H14 000075-83-2.42 Abundance/ Scan 139 (6.318 min): 23797.D (-) m/z 43705 100.00% 4(3 57

71 5000 100

53 6.00 6.20 6.40 6.60 . . ''I l„,... ..... m/z 57.00 86.18% TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Msundance #1528:3-Hexanone 43 57

29 71 6.00 6.20 6.40 6.60 100 m/z 71.00 59.66% ..

t+ ..... I'I t "i""i .. ^l""l tVz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance#63398:.3-Pentanone, 2-methyl------------------------------- 5)7 43 6.00 6.20 6.40 6.60 aSfi m/z 100.05 34.00% 100 71 85 ~ +TPTTTT P"'”'' I'' ’' I Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 L /Kbundance #63324:2,4-Pentanedione T' 6.40—6.60.r~^ Wz 41705 28711%

5000 85; 100

58 72 . ......... "...I +TTrrrrTTT I "I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60

23797.D NP10'3001.M Thu Nov 01 12:03:58 2001 Page 1

NYC-WTC_000089454

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NYC-WTC_000089454Source: NYC Law Department, mirrored locally

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