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GCMS analysis results, sample AD23915, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23915 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067635–000067650

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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Scanned page image, NYC-WTC_000067643
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\OCT1701\23914.D Vial: 12 Acq On : 18 Oct 2001 12:03 am Operator: 209 GALOS Sample : gc/ms unknown Inst s GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.39 0.43 ug/1 43141 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 intative ID MW MolForm CAS# Qual 1 3-Hexanoi^ 100 C6H12O 000589-38-8 74 2 3-Penta^ne, 2-methyl- 100 C6H12O 000565-69-5 38 3 Butaney'2,2-dimethyl- 86 C6H14 000075-83-2 36 4 2,4-P^tanedione_______________ 100 C5H8O2 000123-54-6 12 Abundance / Scan 147 (6.394 min): 23914.D (-) m/z 43.05 100.00% 43 57

71 5000 100

6.00 6.20 6.40 6.60 6.80 I. . , , I TTTTpTTrjTTTTJTTTrpTTTpTTrpTTrp4TtyrrrrpTTr|Tl4TpTrr|7TTTJTTTTJTTTTpTTT|TTTTJTTTTp-rTT i i i i [ i i i i[ m/z 57.00 86.97% 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance

Ja__ #1528:3-Hexanone 57

29 71 5000 6.00 6.20 6.40 6.60 6,80 100 m/z 71.00 61.26%

L, 85 "I"'... +m’ Tlfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Wxindance #63398:3-Pentanone. 2-m8thyl-

43 6.00 6.20 6.40 6.60 6.80 5000 m/z 100.05 36.78% 100 71 85 -t- Tife-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Wjundance #62861: Butane, 2,2-dimethyl- 43 57 6.00 6.20 6.40 6.60 6,80 71 Wz 41.00 26.86% 5000 29

15 Tife-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6:M 6 40 6 60 6 80

23914.D NP101901.M Wed Oct 24 11:14:53 2001 Page 1 NYC-WTC_000067643

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NYC-WTC_000067643Source: NYC Law Department, mirrored locally

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