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GCMS calibration table data, Nov 2001

Machine-extracted title · confidence 100%

Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.

NYC-WTC_000069732–000069741

Folder label: “GCMS Scan X 10/27/01 An 11/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV16 01\LB.D Vial: 9 Acq On : 16 Nov 2001 10:50 pm Operator: 209 GALOS Sample : lb 10/27 Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Ik********************************************************************

Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.80 ug/1 133837 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 •entative ID MW MolForm CAS# Qual 1 2-Hexanojafe 100 C6H12O 000591-78-6 91 2 2-Hexanone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2i 061141-74-0 64 3 Meth^ Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 Abundance Scan 150 (6.424 min): LB.D (-) Wz 43.00 100.“00% 4(3

58 5000

1(» 6.00 6.^ 6.^ 6.^ 6.^ t|,7,r|im|.lllTTT ’’,1 * " I ” 1111' IH "' 11'' I' I''" 1' 1" I Ttttjttttji IriTz 58.00 55.14% TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63387:2-Hexanone 43

58 i 5000 6.00 6.20 6.40 6.60 6.80 100 “Wz 41.00 14.98% 71 W '" I" " I ‘I' I"' h' I -hrrr 1' ’ " I ‘ Tife-> 20 25 30 35 40 45 50 55 60 65 70 TO80 85 90 95 100 105 Abundance #15807:2-Hexanone, 4-hydroxy-5-rnethyl-3-propyl- 4(3

6.00 6.20 6.40 6,60 6,80 5000 Wz 577^0 14.87% 58 27 72 38 , I .1 85 100 Tp-rrTjttT4yTTTTjrrTTT44+tyrTTTpTTyp4+rprTTTpTTTj+tTTp-rTTJTTrr|T^^ ........ Tl/Z-> 20^ 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance Methyl Isobutyi Ketone <40 6.00 6.20 6.40 6.60 6.80 m/z 100.05 12.30%

5000 58

n&-> .. ..1,1,.. I. ... T.. T.. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 A 6,00 A ,,,, I , J , , I 6,20 6.40 , I ,..A, , 6.^ 6.^

LB.D NP103001.M Tue Nov 27 09:52:02 2001 Page 2

NYC-WTC_000069739

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NYC-WTC_000069739Source: NYC Law Department, mirrored locally

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