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GC/MS calibration table for TCLP analysis, Oct 18 2001

Machine-extracted title · confidence 100%

Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.

NYC-WTC_000088491–000088503

Folder label: “GC/MS Scan 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\LB.D Vial: 2 Acq On : 18 Oct 2001 5:09 pm Operator: 209 GALOS Sample : lab blk 10/15 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.48 1.07 ug/1 103630 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanoni 100 C6H12O 00'0591-78-6 91 2 2-HexanQzfe, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 74 3 MethyKZfsobutyl Ketone 100 C6H12O 000108-10-1 47 4 Propanal 58 C3H6O 000123-38-6 47 Abundance Scan 157 {6.479 min): LB.D (-) m/z 42.95 100.00% 43-

58 5000

85 100 AJ ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' 6.20 6.40 6.60 6.80 I,,,I,ll L 71 I I m/z 58.05 55.70% ■n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63384: 2-Hexanone 43

5000 58 6.20 6.40 6.60 6.80 29 m/ Z 57.00 16.32%

Tl/z-> Abundance 20 Ui 30 50 60 71 70 80 85 90 100 100 #11968: 2-Hexanone, 4-hydroxy-3-propyl- 110 120 130 140

43

58 6.20 6.40 6.60 6.80 5000 29 "mTz 41705 15.25%

71 85 100 140 I ' i ' ‘ ' ' I ' ' ' ' I I r-p-rV- I ' ' ' ' I ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ‘ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1526: Methyl Isobutyl Ketone 43 6.20 6.40 6.60 6.80 m/z 100.00 10.69% 5000 58 27 85 100 51 ' I ' ■nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

LB.D NP091101.M Fri Oct 19 10:25:49 2001 Page 2 I

NYC-WTC_000088498

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NYC-WTC_000088498Source: NYC Law Department, mirrored locally

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