Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.92 ug/1 87989 1,4-Dichlorobenzene-d4 11.76
Hit# Of 5 intative ID MW MolForm CAS# Qual
1 2-Hexano: 100 C6H12O 000591-78-6 90 2 2-Hexam .e, 4-hydroxy-5-methyl-3-pr 172 C10H20O2: 061141-74-0 83 3 2-Hexi one, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 Meth- Isobutyl Ketone 100 C6H12O 000108-10-1 58 Abundance Scan 157 (6.480 min): LB.D (-) m/z 42795 100.00% 43
58 5000
71 85 100 6.20 6.40 6.60 6.80 51 I I I m/z 58.05 52777% ■n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556:2-Hexanone 43
58 5000 6.20 6.40 6,60 6.80 "m/z 41.05 15787% 27 I tVz-> 20 30 40 50 1 60 70 80 90 100 110 120 L-. ....... 130 140 Abundance #15807: 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4b .......... ’ '
6.20 6,40 6,60 6.80 5000 "m/z 57.00 13.74% 58 27
Ti/z-> ^bundance 20 Li 30 40 I - ry-n-rt-YT 50 60 J72 70 80 . 1°°........ 90 100 #11968: 2-Hexanone, 4-hydroxy-3-propyl- 110 120 130 140 43 6.20 6.40 6.60- 6.80 ' m/z. 100.05 10.42% 58
L 5000 29
■n/z-> 'I''''I''''II 20 30 40 ,1 T-p-rV- 50 60 70 80 90 100 110 120 130 140 J/ 6.20 6.40 6.60 6.80
LB.D NP091101.M Thu Oct 18 10:43:40 2001 Page 2
NYC-WTC_000088707
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089418
Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
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