GC/MS calibration report for TCLP method, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data Pile : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On ; 16 Oct 2001 4:11 pm Operator: 209 GAL( Sample : lab blk 9/27 Inst : GC/MS 20i Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★ ★if**************************************** * * * * * *********************

Peak Number 3 2-Hexanol Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.51 ug/1 49054 1,4-Dichlorobenzene-d4 11.76 Hit# Of 5 Tentative ID MW* MolForm CAS# Qua!

1 2-Hex^l 102 C6H14O 000626-93-7 83- 2 2-Penranol, 4-methyl- 102 C6H14O 000108-11-2 78 3 2-^xanol, (S)- 102 C6H14O 052019-78-0 64 4 27©utanol 74 C4H1O0 000078-92-2, 50 . Abundance Scan 184 (6.728 min): LB.D (-) m/z 44.95 100.00% 4*"3

5000 / 41 69 6.40 6.60 6.80. 7.00 56 84 87 -p-rrrj-TTiT-rTVTTT-rTT^^^ I 73 m/z 69.00 14.64% 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ^bundance #63584:2-Hexanol 43

5000 J, /p A 6.40 6.60 ' ' 6.80 ' 7.00 m7z 41.05 13.04% 69 19 ^,31 4^, ■ i|rrrr[Tli-|-p'i-iiTi i 11 [ i HI m-rr I I'''' i''' 11'''' I'''' I'"' I' ‘" I '21' I—

JvW tVz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 - 75 -80 -85-90'"95 5K' Abundance #63546: 2-Pentanol. 4-methyl- 4^ ■ ■■■

6.40 6.60 6.80 7.00' 5000 m/z42.95 11.98% ■■ -

27 69 42 57 I W87 . 'Y-■ I 1 1 • 11 ‘ " 11 H I 1 I I ■ ■ 11 ■ I ■ ’ I

TlZZ-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 ,85 -90 -95- Abundance ._ . #1769:2-Hexanol, (S)- T ------------------ * .-4(5----- - ----- —— - 6.40 6.60 6.80 7.00 • m/ z 43.95 10.52%

5000

55 1 8487 I 1 I I I I 1 I I 11 I I I I H I I 1 I I ) 11 I I I I I I I I H I 1 I U I 1 I I 1 I I I I Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

LB.D NP091101.M Thu Oct 18 10:43:42 2001

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