Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound-Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GTkLOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T.
11.62 0.52 ug/J<' 49616 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 1,4-DicJi<lorobenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzepevl,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 IH- rrolo[2,3-b]pyridine-2,6-dione 152 C7H8N2O2 017384-56-4 9 4 Biy .enylene 152 C12H8 000259-79-0 9 Abundanre Scan 717 (11.621 min); LB.D -) m/z 149.90 rW./m 1$0 A
5000 115 52 ™ T 207 11.20 11.40 11,60 11.80 12.00 T tX T' '■'‘’I’ "m7z’T^5T790 66757% n/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 A Abundance #9593; 1,4-Dichlorobenzene-d4 J 1$0
5000 115 78 11.20 11.40 11,60 11.80 12.00 52 m/z 114.90 38.87% ... 35 .......................... ,i,i„..... ............... . A 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #9592; Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0 ' ’ I ' ' 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 “mTz 77795 21.36%
87 2= J_ 1 [n/^-> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 pT--r-r-r-p--r-r-r^i=rT-/-rp>T-r-r^^ Abundance #10125; 1 H-Pyrrolo[2,3-b]pyridine-2,6-dione, 3,3a,4,5-tetta _ _ -- I- - -------------------------------- J $2 - 11:20-'11:40- 11.60 11.80 12.00 109' -- ------------------- “m/z 52.00 . 15.16% 53 5000 80 27 67 .... I. -37 1(124 YpTTryrnYp T" " I " " 1111 11111 11 111 ■ 1' r' ' hTZz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 11,20 11.40 11.60 11.80 12.00
LB.D NP091101.M Thu Oct 18 10:43:44 2001 Page 4
NYC-WTC_000088709
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
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