GC/MS analysis report with TCLP calibration table data from October 16, 2001.
NYC-WTC_000089030–000089044Folder label: “GC/MS Scan 9/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator: 209 GALOS Sample : lab blk 9/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.52 ug/1 56902 1,4-Dichlorobenzene-d4 11 .'76
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzj^e-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1,2,3,^d4-, 5,6-dichloro- 150 C6C12D4 . 002199-69-1 32 3 BenzaldehydeyY2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 2-Methyl-6-B(itroaniline 152 C7H8N2O2 000570-24-1 10 Abundance Scan 717 (11.626 min): LB.D (-) m/z 149.90 100.00% 1!i0
5000 115 52 78 T'"''' I ■ " I n L2 38 45 I , 63 I 87 11.20 11.40 11.60 11.80 12.00 ' ' I ' ' ' H I m/z 151.90 . 62.79% nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150
5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 . 33.17% TT^,-,-,-r,,ll|,M'y|i,,i|.......... rU............................ 35 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3.4-d4-, 5,6-dichloro- 150
115 11.20 1140 11^60 11.80 12.00 5000- 52 78 "m/z 77795 18.60%
87
T\IZ-> 30 35 I ' I ' ' ' ' I 40 _ I ' ' ' ' I ' ' ' ' I ' 50 60 70 ' I ' ' ' ' I ' ' ' ' I ' 80 90 100 3^ 110 120 130 140 150 160 4..,. ^bundance ------ #66892: Benzaldehyde. 2-hydroxy-3-methoxy- —152? 11:20-11.40 -11.60-1.1.80-12.00-- ■"m/z 51.90 16.19% 106 5000 53 81
' I'''' I *'' * I 111111' ■ I ■' 111' 122 136 I ' I '' ' ' I ' ‘ ' I nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00
LB.D NP091101.M Tue Oct 16 15:20:40 2001 Page 8 ‘4 NYC-WTC_000089043
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NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087496
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000089025
Fragmented GC/MS scan page from a laboratory blank sample dated September 28, 2001.
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NYC-WTC_000089026
Fragmented GC/MS scan page from a laboratory blank sample dated September 28, 2001.
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NYC-WTC_000089045
Laboratory report documenting GC/MS analysis of sample AD23652 conducted on October 16, 2001.
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NYC-WTC_000089059
Laboratory report documenting GC/MS analysis of sample AD23651 conducted on October 16, 2001.
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NYC-WTC_000089073
Laboratory record for sample AD23653 showing detection of unknown compounds on October 16, 2001.
Filed in the same folder