GC/MS chromatogram data for lab blank 9/25, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\LB.D Vial: 12 Acq On : 12 Oct 2001 12:53 pm Operator: 209 GALOS Sample : lab blk 9/25 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.55 ug/1 88093 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tent^ive ID MW MolForm CAS# Qual 1 1,4-Dichloro: enzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2/ ,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 43 3 Benzaldeh; e, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 Benzofur/ , 7-chloro- 152 C8H5C1O 024410-55-7 9 Abundance Scan 716 (11.617 min): LB.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 40 , 87 11.20 11.40 11.60 11.80 12.00 ....... m/z 151.90 61.51% ■n/z-> 30 40 50. 60I 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 34.31% 35 ...... 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0 T-n-p-i f I p I I I I I I

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 "m/z 78.05 20.50%

87

Tife-> 30 35 I 40 50 60 70 80 I 90 100 110 120 130 A 140 150 160 Jlu, Abundance #66892: Benzaldehyde, 2-hydroxy-3-niethoxy- 1!!2 11.20 11.40 11.60 11.80 12.00 “mTz 52.00 16.79% 106 553 53 81

92 122 136 ' 1111111 11 ' 11 ' 11''' I' ' I ' ‘ ‘ ' I ' ' ' ' I T ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

LB.D NP091101.M Mon Oct 15 15:00:42 2001 Page 3

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