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← Document results/DEP Box 60/GCMS Scan X 10/2/01 An 10/17/01
Document / 11 pages

GCMS calibration table, Oct 17 2001

Machine-extracted title · confidence 90%

Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.

NYC-WTC_000067428–000067438

Folder label: “GCMS Scan X 10/2/01 An 10/17/01”

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Scanned page image, NYC-WTC_000067437
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\OCT1701\LB.D Vial: 2 Acq On : 17 Oct 2001 2:09 pm Operator; 209 GALOS Sample : lab blk 10/2 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.54 ug/1 57880 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-DichlorobeXzene-d4 150 C6C12D4 003855-82-1 91 2 Benzene-1,2^3;4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 9 4 2H-l-Bep^pyran-3-ol, 3,4-dihydro- 150 C9H10O2 021834-60-6 9 ^bundance / Scan 717 (11.620 min): LB.D (-) m/z 149.90 100.00% 1ii0

5000 115 78 52 ii'^' '11'40' ‘1'1 .eo' Vtso' lalob' 40 ' ‘ I' ‘' I ‘' m/z 151.90 66.46% TiZz-> 30 40 K) 60 70 80 90 100 110 120 130 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 I ' ‘ ' 1 ‘ ‘ ' 1 ' ‘ 78 11.:y 11.40 11,60 11.80 12.00 52 m/z 114.90 35770%

Tife-> 30 35 40 50 60 70 80 90 I ' ' ' ’ 1 100 110 120 130 140 150 160 ku. Abundance #9592: Ben2ene-1,2,3.4<l4-, 5.&<lichloro- liiO

115 11.^ 11.40 11.60 11.80 12.00 5000 52 78 "mTz 78.05 24.43%

87

■n&-> 30 35 I ‘ I'''' I 40 50 ''' I' 60 70 I ' I'''' I ■ 80 90 100 110 120 130 A 140 150 160 Mxindance #66892: Benzaldehyde. 2-hydroxy-3-methoxy- 112 irz) '1'1'40' '1'1 So' ii!m 'izro ■m/z 52.00 . 14.06% 106 5000 53 81

122 ■ I • •' • 11 • 1 ■ 11 92 I I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

LB.D NP101901.M Tue Oct 23 12:52:55 2001 Page 4 NYC-WTC_000067437

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NYC-WTC_000067437Source: NYC Law Department, mirrored locally

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Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

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