Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
NYC-WTC_000067428–000067438Folder label: “GCMS Scan X 10/2/01 An 10/17/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File s C:\HPCHEM\1\DATA\OCT1701\LB.D Vial: 2 Acq On : 17 Oct 2001 2:09 pm Operator; 209 GALOS Sample : lab blk 10/2 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.54 ug/1 57880 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-DichlorobeXzene-d4 150 C6C12D4 003855-82-1 91 2 Benzene-1,2^3;4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 9 4 2H-l-Bep^pyran-3-ol, 3,4-dihydro- 150 C9H10O2 021834-60-6 9 ^bundance / Scan 717 (11.620 min): LB.D (-) m/z 149.90 100.00% 1ii0
5000 115 78 52 ii'^' '11'40' ‘1'1 .eo' Vtso' lalob' 40 ' ‘ I' ‘' I ‘' m/z 151.90 66.46% TiZz-> 30 40 K) 60 70 80 90 100 110 120 130 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0
5000 115 I ' ‘ ' 1 ‘ ‘ ' 1 ' ‘ 78 11.:y 11.40 11,60 11.80 12.00 52 m/z 114.90 35770%
Tife-> 30 35 40 50 60 70 80 90 I ' ' ' ’ 1 100 110 120 130 140 150 160 ku. Abundance #9592: Ben2ene-1,2,3.4<l4-, 5.&<lichloro- liiO
115 11.^ 11.40 11.60 11.80 12.00 5000 52 78 "mTz 78.05 24.43%
87
■n&-> 30 35 I ‘ I'''' I 40 50 ''' I' 60 70 I ' I'''' I ■ 80 90 100 110 120 130 A 140 150 160 Mxindance #66892: Benzaldehyde. 2-hydroxy-3-methoxy- 112 irz) '1'1'40' '1'1 So' ii!m 'izro ■m/z 52.00 . 14.06% 106 5000 53 81
122 ■ I • •' • 11 • 1 ■ 11 92 I I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00
LB.D NP101901.M Tue Oct 23 12:52:55 2001 Page 4 NYC-WTC_000067437
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NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000067405
Record of a GCMS scan conducted at the World Trade Center site between October and November 2001.
Filed in the same folder
NYC-WTC_000067406
Gas chromatography-mass spectrometry analysis of sample AD22558 started October 1, 2001, identifying other unknown compounds.
Filed in the same folder
NYC-WTC_000067425
Log sheet recording liquid-liquid extraction parameters and sample processing details for October and November 2001.
Filed in the same folder
NYC-WTC_000067439
DEP lab report for GCMS analysis of sample AD23844 conducted on October 23, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067453
DEP lab report for GCMS analysis of sample AD23900 conducted on October 23, 2001, noting unknown compounds.
Filed in the same folder