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Document / 13 pages

GCMS calibration table for TCLP analysis, Oct 25 2001

Machine-extracted title · confidence 95%

Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.

NYC-WTC_000067739–000067751

Folder label: “GCMS Scan X 10/5/01 An 10/25/01”

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Scanned page image, NYC-WTC_000067750
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\LB.D Vial: 2 Acq On : 25 Oct 2001 11:58 am Operator: 209 GALOS Sample : lab blk 10/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.59 0.54 ug/1 92664 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenz .e-d4 150 C6C12D4 003855-82-1 94 2 Benzene-1,2z3,4V 5,6-dichloro- 150 C6C12D4 002199-69-1 37 3 Biphenylene / 152 C12H8 000259-79-0 9 4 Benzaldehyde,/2- hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 9 ^bundance Scan 713 (11.592 min): LB.D (-) m/z 149.90 100.00% 1!i0 /

5000 115 52 78 -f 40 11.^ 11.40 11.60 11.80 12.00 ■ l-l I >■- TTTTrHr 1 ‘ ‘ ' I 4^ m/z 151.90 60.16% Tl/Z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichloroben2ene-d4 liW

5000 115 T 78 11.^ 11.40 11.60 11.80 12.00 52 m/z 114.90 39.75% (1 35 I ' ' ' ' I TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3.4-d4-, 5.6-dichloro- ISO T T R 11.^ 11.40 11.60 11.80 12.00 115 5000 52 78 m/z 78.05 21.12%

87

n/z-> 30 35 I 40 50 60 70 I ' I'''' 1' 80 90 100 110 A I 120 130 140 150 160 T

^bundance #67017: Biphenylene T 1!2 11.^ 11.40 11.60 11.80 12.00 m/z 52.00 18.61%

5000

63 76 126 1 97 -W|+TTT-p--r-r-r-p- I ‘ ' I T 30 40 50 60 70^80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

LB.D NP101901.M Mon Oct 29 09:51:56 2001 Page 6

NYC-WTC_000067750

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NYC-WTC_000067750Source: NYC Law Department, mirrored locally

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