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GCMS analysis results for sample AD25041, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25041 conducted on November 19, 2001, identifying unknown compounds.

NYC-WTC_000069256–000069266

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069265
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\25041.D Vial: 15 Acq On ; 9 Nov 2001 4:16 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.52 ug/1 109635 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tent ive ID MW MolForm CAS# Qual 1 1,4-Dichlorob zene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2, , 4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 37 3 Biphenylene 152 C12H8 000259-79-0 9 4 Benzofuran 7-chloro- 152 C8H5C1O 024410-55-7 9 Abundance / Scan 712 (11.578 min): 25041 .D (-) m/z 149.90 100.00% liiO

5000 115 52 78 11 20 11,40 11.60 11.80 12.00 40 ... H'L,, m/z 151.90 I 67.80% mZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

..... 5000 115 78 11.20 11,40 11.60 11.80 12.00 52 m/z 114.90 35.93%

■nfe-> 30 35 40 50 60 4V4 70 80 100 90 110 1 20 130 140 150 160 Abundance #9592: Benzen6-1,2,3,4-d4-, 5,6-dichloro- 1!i0 . ......... / V...... 115 11 20 11,40 11.60 11.80 12.00 5000 52 78 m/z 78.05 19.88%

35 I ... .,1,1.... tVz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67017: Biphenylene .T'. /' ' V' I 152 11 20 11.40 11,60 11,80 12.00 m7z 52.00 17.39% 5000

63 76

30 40 50 4^ 80 90 97100 110 120?130 60 70 ' I ' '' ' I ' ' ''''I I ' . ' I ' . i I I ■ .1' I ■ 140 150 160 r _____ 11.20 11.40 11.60 11,80 12.00

25041.D NP103001.M Mon Nov 19 12:12:05 2001 Page 2 NYC-WTC_000069265

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NYC-WTC_000069265Source: NYC Law Department, mirrored locally

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