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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 11.64 0.52 ug/1 69364 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 91 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 3 Biphenylene 152 C12H8 000259-79-0 10 4 Benzofuran, 7-chloro-____________________ 152 C8H5C1O 024410-55-7 10 Abundance Scan 719 (11.641 min): 22546. D (-) m/z 149.90 100.00% 1!i0

5000

52 78 115

ill,,.?,....... J).... ........ I. u' I ' 11.40 11.60 11.80 12.00 m/z 151.90 59.42% 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000- 115 T T 78 11.40 11.60 11.80 12.00 52 m/z 115.00 35.21% 35 I ’ ' ' ' I Tl/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0

115 11.40 11.60 11.80 12.00 5000 52 78 m/z 77.95 17.18%

35 87

m/z-> 30 I 40 50 60 70 I 80 90 A .. 100 110 120 130 140 150 160 Abundance #10447: Biphenylene 152 11.40 11.60 11.80 12.00 m/z 52.00 13.33%

5000 ft 63 76

n/z-> 30 40 50 60 70 80 87 90 98 -h- 126

100 110 120 130 140 150 160 I '' ' ' I A 11.40 11.60 11.80 12.00

22546.D NP091101.M Wed Oct 03 14:44:31 2001 Page 4

NYC-WTC_000086960

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NYC-WTC_000086960Source: NYC Law Department, mirrored locally

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