GCMS analysis results for sample AD26205, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26206.D Vial: 56 Acq On : 30 Nov 2001 8:34 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.57 ug/1 128733 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Ten' tive ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2, 3, 4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 23 3 Benzofuran, 7-chloro- 152 C8H5C10 024410-55-7 9 4 Biphenylene 152 C12H8 000259-79-0 9 Abundance 7 Scan 710 (11.559 min): 26206.D (-) m/z 149.90 100.00% 150

5000 115 .................... — 52 78 38 87 11.20 11.40 11.60 11.80 38 45 45 , , ,59 66 — —........... 'll —HHir — mpur 1’l• m/z 151.90 66.84% miz-> 30 40 50 60 70 80 90 100 1W 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

• i • • ■ ■ i— — 5000 115 78 11.20 11.40 11.60 11.80 52 m/z 114.90 38.22% 35 87 L ■ ■ i ■ ‘■ i ■ ■ ‘ ■ i • • । • ■ • ■ ।* —T —1100200 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-44-, 5,6-dichloro- 150 —II_ mp— 1 r Ip 1 I_ 1_ I_ I_ r 11.20 11.40 11.60 11.80 115 5000 52 78 m/z 77.95 22.02%

35 87 | ■ ■ i ■ ■ ‘ ■ i1 ■ ‘ ■ i ■ ■ । ■111 •1 i ■ ■ ■ ■ i +4 I ‘ ‘ 1 * ! • • । ■ mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10136: Benzofuran, 7-chloro- 152 11.20 11.40 11‘BO 11.80 * ■ i • m/z52.00 , 15.99% 5000 89

63 35. .-j-r-n-r 49 73 125 . , । — — 11111111111100100‘‘I L ‘ II 1T T 1" m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

26206.D NP112601.M Mon Dec 03 09:42:06 2001 Page 3

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