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GCMS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 90%

Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.

NYC-WTC_000068559–000068571

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0501\LB.D Vial: 2 Acq On : 5 Nov 2001 12:14 pm Operator: 209 GALOS Sample : 10/16 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 94581 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 T^tative ID MW MolForm CAS# Qual

1 l,4-DichloB6benzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-]y2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 2-Methy/- 6-nitroaniline 152 C7H8N2O2i _______000570-24-1 10 Abundance Scan 711 (11.569 min): LB.D {-) m/z 149.90 100.00% 1!i0

5000 115 52 78

Ti^-> 30 UuuUs ... 1.1,..y.......... . 40 50 60 70 80 ......... H'L,, ,| 90 100 110 120 130 140 150 160 1t201140116011J0 m/z 151.90 62.39% Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 ' I ' ' ' ' 1 ' ' 78 1120 11.40 11,60 11.80 52 m/z 114.90 33.89%

Ti^-> 30 35 40 50 60 UUn 70 80 90 100 110 120 130 - 140 150 160

.... J\.. Abundance #9592: Benzene-1.2.3,4-d4-, 5,6-dichloro- 1!i0

115 11.20 11.40 11.60 11.80 5000 52 78 m/z78.05 18.93%

35 87 I ' I ' ' '' I '' ' ' I ' ' ' ' I ' I ' I'''' I' ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 11.20 11.40 11.60 11.80 m/z 52.00 15.87% 106 5000 53 81

■nZz-> 30 40 50 60 70 80 92 'H' 90 100 110 120 122

130 136 140 p I 150 160 ... JU 11.20 11.40 11.60 11.80 ____

LB.D NP103001.M Fri Nov 09 12:14:21 2001 Page 6

NYC-WTC_000068570

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NYC-WTC_000068570Source: NYC Law Department, mirrored locally

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