Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
NYC-WTC_000068559–000068571Folder label: “508 Scan X 10/16/01 A 11/5/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV0501\LB.D Vial: 2 Acq On : 5 Nov 2001 12:14 pm Operator: 209 GALOS Sample : 10/16 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 1.55 ug/1 276079 1,4-Dichlorobenzene-d4 11.72
Hit# Of 5 "entative ID MW MolForm CAS# Qual
1 2-Pent ano: , 4-hydroxy-4-methy1- 116 C6H12O2 000123-42-2 50 2 Acetic ao■id, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 5-Hexen^ -one 98 C6H10O 000109-49-9 9 4 Acetoner 58 C3H6O _______000062^6121 9 Abundance Scan 289 (7.695 min); LB.D (-) Wz 42.95 100.00% 43
59 5000
101 7.40 7.60 7.80 8,00 . ......... +-r ......................... 1,1........ m/z 59.05 50.46% 'nlz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- 43
5000 59 7.40 7.60 7.80 8.00 m/z 101.05 22.39% 31 I I
n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethyiethyl ester 43
7.40 7.60 7.80 8.00 5000 57 m/z 58.05 16.55% 101 15 27 I ' I' ' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ ' I ' ‘ ' 1 Ti/z-> 10 20 30 40 60 70 80 90 100 110 Abundance #63205:5-Hexen-2-one 43 7.40 7.60 7.80 8.00 m/z 41.05 8.22%
5000
55 15 27 I I 38 I 50 I 83 98 1 ‘ ' I ' ' ' ' I ' I • ' ' ’ 1~' ' I ' ' ' ' I ' ' ' ' I ' ■ I 1 I • • ■ I 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
LB.D NP103001.M Fri Nov 09 12:14:19 2001 Page 5
NYC-WTC_000068569
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NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
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Log sheet recording liquid-liquid extraction parameters and sample processing details for November 2001.
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Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
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NYC-WTC_000068585
Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.
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Laboratory report documenting GCMS analysis of sample AD24489 conducted on November 13, 2001, identifying unknown compounds.
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