Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
NYC-WTC_000068559–000068571Folder label: “508 Scan X 10/16/01 A 11/5/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV0501\LB.D Vial: 2 Acq On : 5 Nov 2001 12:14 pm Operator: 209 GALOS Sample : 10/16 lab blk Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclotrisiloxane, hexamethyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.16 0.60 ug/1 106309 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclatrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 80 2 ArOUS acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 50 3 1^Indole, 5-methyl-2-phenyl- 207 C15H13N 013228-36-9 38 4 4“Indole, 1-methy1-2-phenyl- 207 C15H13N 003558-24-5 38 \bundance Scan 231 (7.163 tnin): LB.D (-) m/z 207.00 100.00% 2(1)7
5000
u I' " ' I " " I' ' " I " ' ' I 6.80 m/z 208.00 7.00 n 7.20 7.40 7.60 19.90% Tite-> Wjundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 #27918: Cyclotrisiloxane, hexamethyl- 207 (V 5000 ‘ ' I ' ' ‘ ‘ I ' ' H ‘ ‘ ' 6.80 7.00 7.20 7.40 7.S m/F 95.90 15.78% 73 .T.115;?^ 163,T ttZz-> 15 20 40 60 ' ' I ’ ' 1' I ' ' '' I ' ' ' ' I' I ' ' ' ' 80 100 120 140 160 180 200 220 240 260 280 300 320 4^ I' ' ' ' I '' ' ' I ' ' '' I ' ' ' ' I
Abundance #48300: Arsenous acid. tris(trimethylsilyl) ester 207
6.80 5000 m/z 208.90 13.59%
n/z-> Abundance
5000 ''' I' ‘' I'' 20 40 44 60 73 II 105 133 191 Il 223239 * « I ' * ' I I H I I I I I I « I 80 100 120 140 160 180 200 220 240 260 280 300 320 #24654: IH-lndole, 5-methyl-2-phenyl- 207 327 I' '
6.80 m/z 191.00 7.00 h 7.20 7.40 9.04%
Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 6.80 7.00 7.20 7.40 7.60
LB.D NP103001.M Fri Nov 09 12:14:17 2001 Page 4
NYC-WTC_000068568
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NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000068555
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
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NYC-WTC_000068556
Log sheet recording liquid-liquid extraction parameters and sample processing details for November 2001.
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NYC-WTC_000068572
Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
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NYC-WTC_000068585
Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.
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NYC-WTC_000068598
Laboratory report documenting GCMS analysis of sample AD24489 conducted on November 13, 2001, identifying unknown compounds.
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