NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D Vial; 11
Acq On : 17 Oct 2001 12:01 am Operator; 209 GALOS
Sample : gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params; LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
**************** '*****************************************************
Peak Number 4 Cyclotrisiloxane, hexamethyl- Concentration Rank 19
R.T. EstConc Area Relative to ISTD R.T.
.7.21 0.53 ug/1 50802 1,4-Dichlorobenzene-d4 11.76
Hit# of 5 intative ID MW MolForm CAS# Qua!
1 Cyclotri^ oxane^^examethyl - 222 C6H18O3Si3 000541-05-9 86
2 Arsenou^^ TdTTris (trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 56 \
3 IH-m^le, 1-methyl-2-phenyl- 207 C15H13N 003558-24-5 45 '
4 IH-I/bindole-l,3(2H)-dione, 2-butyl 207 C12H17NO2 054934-85-9 40
Abundance/ Scan 236 (7.211 min); 23503.D (-) m7z207700100.00%
207
5000
96 I
75 I 119133147 163177’'®’' | 6.80 7.00 7.20 7.40 7.60
45
'' I"''''' I' pnrT-rpnnr7Tq~r-T-T-Ty-^^ m/z 208.00 23.15%
-n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320
Abundance #70586: Cyclotrisiloxane, hexamethyl-
2(1)7
6,80 7.00 7.20 7.40 7.60
77
m/z 96700 17749%
75 119'’^3i47 ira177^f/
' ’ I ' ' ' I I • • ’ ' I ' ' ' ' IV. I • I I I fI I I ' ' ' ' I • ' ' ’ I ' " ' I " ‘ ' I ' ' ' ' I
n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320
Abundance #48300: Arsenous acid, tris(trimethylsilyl) ester
2(1)7 ------- ------- —■
6.80 7.00 7.20 7.40 7.60
5000 m/z 209.00 12711%
105 133...,
44 7 I I, 147
] V .1 I I ri i"|-pr'r.
191 223 239
T-p-n-rp-
327
‘ ' I
nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320
Abundance #24655: IH-lndole, 1 -methyl-2-phenyl-
2(1)7 6.80. 7.00—7.20 7.40 7.60
-m/z -190V90 9.12%
5000-
nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320
I ' ' ' * I ' ' ' ' 1 ' ' ' ' 1 ' ' ' ' I
6.80
- -IK
7.00 7.20 7.40 7.60
23503.D NP091101.M Thu Oct 18 10:28:48 2001 Page .4
NYC-WTC_000088915
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