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GC/MS analysis results for sample AD23503, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.

NYC-WTC_000088905–000088934

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088915
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D Vial; 11 Acq On : 17 Oct 2001 12:01 am Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L **************** '***************************************************** Peak Number 4 Cyclotrisiloxane, hexamethyl- Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. .7.21 0.53 ug/1 50802 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 intative ID MW MolForm CAS# Qua!

1 Cyclotri^ oxane^^examethyl - 222 C6H18O3Si3 000541-05-9 86 2 Arsenou^^ TdTTris (trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 56 \ 3 IH-m^le, 1-methyl-2-phenyl- 207 C15H13N 003558-24-5 45 ' 4 IH-I/bindole-l,3(2H)-dione, 2-butyl 207 C12H17NO2 054934-85-9 40 Abundance/ Scan 236 (7.211 min); 23503.D (-) m7z207700100.00% 207

5000

96 I 75 I 119133147 163177’'®’' | 6.80 7.00 7.20 7.40 7.60 45 '' I"''''' I' pnrT-rpnnr7Tq~r-T-T-Ty-^^ m/z 208.00 23.15% -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #70586: Cyclotrisiloxane, hexamethyl- 2(1)7

6,80 7.00 7.20 7.40 7.60

77 m/z 96700 17749% 75 119'’^3i47 ira177^f/ ' ’ I ' ' ' I I • • ’ ' I ' ' ' ' IV. I • I I I fI I I ' ' ' ' I • ' ' ’ I ' " ' I " ‘ ' I ' ' ' ' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #48300: Arsenous acid, tris(trimethylsilyl) ester 2(1)7 ------- ------- —■

6.80 7.00 7.20 7.40 7.60 5000 m/z 209.00 12711%

105 133..., 44 7 I I, 147 ] V .1 I I ri i"|-pr'r. 191 223 239 T-p-n-rp- 327 ‘ ' I nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #24655: IH-lndole, 1 -methyl-2-phenyl- 2(1)7 6.80. 7.00—7.20 7.40 7.60 -m/z -190V90 9.12% 5000-

nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 I ' ' ' * I ' ' ' ' 1 ' ' ' ' 1 ' ' ' ' I 6.80 - -IK 7.00 7.20 7.40 7.60

23503.D NP091101.M Thu Oct 18 10:28:48 2001 Page .4

NYC-WTC_000088915

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NYC-WTC_000088915Source: NYC Law Department, mirrored locally

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