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GCMS analysis results for sample AD24287, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24287 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068117–000068130

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068126
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NYC 9/11 Public Portal Document

Library Search Compound Report Data Pile : C:\HPCHEM\1\DATA\OCT3101\24238.D Vial: 5 Acq On : 31 Oct 2001 8:01 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P •Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L A******************************************************************** Peak Number 2 Cyclotrisiloxane, hexamethyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.16 0.55 ug/1 77080 1,4-Dichlorobenzene-d4 11.71 Hit# of 5^__j:gi^ative ID MW MolForm CAS# Qual 1 CyclotrIsiloxaneJ hexamethyl- 222 C6H18O3Si3 000541-05-9 90 2 Arsenou tris (trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 39 3 IH-Indole, 2-methyl-3-phenyl- 207 C15H13N 004757-69-1 9 4 IH-Indole, 1-methyl-2-phenyl- 207 C15H13N 003558-24-5 9 Abundance 230 (7?159 min): 24238.D (-) m/z 206.95 100.00% 2(1)7

5000

, , 42 59 75 I j..... 6.80 7.00 7.20 7.40 7.60 m/z 208.00 19.66% nfe-> aSoi" ' ot" ' ro' 'i6o' 'i'^' ‘i4o‘ 'i^' iro' ‘2^' 3^' Abundance #70586: Cydrtrisiloxane. hexamethyl- 2(b7

5000 6.80 7.00 7.20 7.40 7.60 raTz 95.90 14777% 96 75 ■ ■T i19Ti47 163177 [ -TTp-TT+jTTTT-'l-TTTh-pTT-rjYTT^^ n* ’ ‘ I p •»• I •' ‘' I Ti&-> 20 40 60 80 100 1g) 140 160 180 200 220 240 260 280 300 320 <U)undanc8 #48300: Arsenous acid, tris(trimethylsilyl) ester 207

'e.^' '7.06' '7.^' ‘7.^ zro m/z 209.00 13.45%

,h 5000

73 105 133,.., 191 44 I I, 147 223239 327 I"''I Tym-rp- 111 ■ I ]. I r. 11111 ] P' ’ nZz-> M40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #24658: IH-Indole, 2-methyl-3-pheny)- 2(17 _j6^g_Z00_^,^_^40_7^ m/z 190.90 11.29% 5000

130 30 Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 6.80 7.00 7.20 7.40 7.60

24238.D NP103001.M Fri Nov 02 11:58:47 2001 Page 2

N YC-WTC_000068126

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NYC-WTC_000068126Source: NYC Law Department, mirrored locally

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