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GCMS analysis results for sample AD24287, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24287 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068117–000068130

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068125
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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24238.D Vial: 5 Acq On : 31 Oct 2001 8:01 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.74 ug/1 103259 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexi me 100 C6H12O 000591-78-6 91 2 Oxira: , 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 72 3 2-He: .none, 4 - hydroxy - 3 - p ropy 1 - 158 C9H18O2 062338-17-4 64 4 Met 1 Isobutyl Ketone 100 C6H12O 000108-10-1 52 Scan 149 (6.416 min): 24238.D (-) m/z 4279^5 100.00% 43

58 5000

''1....... 41 51 T-p-T*T I, 71 86 IMIMI^ 6.00 m/z 6.^ 58.00 6.40 6.60 58734% 6.80

TiZz-> 20 30 40 50 60 70 80 90 100 110 Abundance #63387:2-Hexanone 43

58 5000 r • • ■ • I ■' I. ■ I ■ ' I ' ■ ' 6.00 6.20 6.40 6.60 6.80 100 m/z 57.00 18.08% 71 85 I I • I • • ■ ' 1 ' ■ • I ■ 1 • ■ ■ 11' ’ ■ • I' Tife-> 20 30 40 50 60 70 80 90 W01101M1M140 Abundance #1530: Oxirane. 2-methyl-2-(1-methylethyD- 4(3 58 6.00 6.20 6.40 6.60 6.80 50CX) "mTz 41.05 14.47% 71

30 85 100 rTT-rVi-p-rT-rlTT-TTTT-T^^ 1'' *' I ' Tlfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968; 2-Hexanone, 4-hydroxy-3-propyI- 43 6.00 6.20 6.40 6.60 6.80 58 m/z 99.95 12.36% 5000

nZz-> 29

' I ■ ‘'' I' ''' I ' 20 30 40 J. ' I' ' ■ 50 60 71 I ‘' I ‘ 70 I ' I ' 80 85 100 .1,................. 90 100 110 120 130 140 140 wu 6.00 6,20 .i,6.40 6.60 6.80

24238.D NP103001.M Fri Nov 02 11:58:45 2001 Page 1

NYC-WTC_000068125

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NYC-WTC_000068125Source: NYC Law Department, mirrored locally

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