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GCMS analysis results for sample AD23997, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23997 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067782–000067795

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23997.D Vial: 5 Acq On : 25 Oct 2001 4:36 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.47 0.85 ug/1 166287 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone / 100 C6H12O 000591-78-6 91 2 Oxirane, 2/methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 78 3 Methyl Ixobutyl Ketone 100 C6H12O 000108-10-1 58 4 2-Hexaqone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 Abundance Scan 155 (6.465 min): 23997.D (-) m/z 42.95 100.00% 4(3

58 5000

6.20I 6.40 6.60 6.80 51 .. ........ .T..I p m/z i58.05 55.22% TiZz-> 20 253035404550556065 70 75 80859095 100 105 Abundance #63386:2-Hexanone 43

5000 58 I A ■ ■ p 1 • ■ • I I PPTT 71..^ 6.40 6.60 6.80 29 m/z ;57.00 17.16% 71 85 I" " I' 1111" " I TtTTTyrTTTp-rTTj-rTT-rpTT-rpT-rT^TTTrp-rrrp ’' I ’ “ ' I' +t TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1530: Oxirane, 2-methyl-2-(1 -methylethyl)- 4t3 58 6.20 6.40 6.60 6.80 5000 "mTz 16757% 71

30 66 85 100 11■'11 I Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 '\bundance #63351: Methyl Isobutyl Ketone 4(3 " ' 6,^ " 6.^ " 6.CT " 6.ro' m/z 100.05 10.45% 5000

rnfe-> 27 I ‘' I' I ‘' I"' ‘ I 20 25 30 35 40 45 50 55 OTKTOTOSOSS M^IOOire 58 85 100 . , 1'7.. 6.2) 6.40 6.60 6.80

23997.D NP101901.M Fri Oct 26 10:10:57 2001 Page 2

NYC-WTC_000067791

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NYC-WTC_000067791Source: NYC Law Department, mirrored locally

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