GCMS analysis results for sample AD26008, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26008 conducted on December 12, 2001.

NYC-WTC_000030864–000030874

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\NOV1901\26008 . D Vial: 18 Acq On : 20 Nov 2001 7:54 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclotrisiloxane, hexamethyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.15 0.48 ug/1 99489 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotrisiloxane, hexamethyl- 222 C6H1803Si3 000541-05-9 72 2 Arsenous d, tris(trimethylsilyl) 342 C9H27As03Si3 055429-29-3 56 3 lH-IndoLe, 5-methyl-2-phenyl- 207 C15H13N 013228-36-9 45 4 1H-Indol e, 1-methyl-2-phenyl- 207 C15H13N 003558-24-5 39 Abundance Scan 230 (7.154 min): 26008.D (-) m/z 207.00 100.00% 207

5000 -

96 — I nc 133 6.80 7.00 7.20 7.40 1 40 55 75 | 115 । "I.. . "1TI1 THT 177121 ।. A,.. ? 111 r> 111111 TVTTTTT 1111 ■ । IT 1111111 m/z 208.00 22.58% m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #27918: Cyclotrisiloxane, hexamethyl- 267

5000 IT 6.80 7.00 7.20 7.40_____ 96 133 m/z 96.00 16.89% . 15 73 | 115 133 163 , 191

N, — 222 DT "II I' •' ’ I ITT TUIg] ■ i' ■ ■ • i i •1111 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #48300: Arsenous acid, tris(trimethylsilyi) ester 207

6.80 7.00 7.20 7.40

M 5000 m/z 208.9013.05%

73 105 133 44 191 223 239 327 1111'11 ■ ■" i1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 'Abundance #24654: 1H-lndole, 5-methyl-2-phenyl- ■ • i • 207 6.80 7.00 7.20 7.40 m/z M 9.13W 5000

m/z-> ............. 104128 152 ..... ...... ' l' " ' I' 1 " I 1 1 " I' ' “ l 1 TT—0110"TTTT1IT ‘T . ′′ 'i11 ' ■ । ‘ ‘ | " " I' 11 'T'' " I 1'1 111 1 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 — ——————— 6.80 7.00 7.20 7.40 |

26008.D GCMS1126.M Wed Dec 12 09:51:53 2001 Page 1

NYC-WTC_000030872

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