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GCMS analysis results for sample AD26008, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26008 conducted on December 12, 2001.

NYC-WTC_000030864–000030874

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV1901\26008.D Vial: 18 Acq On : 20 Nov 2001 7:54 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\l\METHQDS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.70 1.17 ug/1 240676 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetic acid , 1,1-dimethylethyl este 116 C6H1202 000540-88-5 33 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 5-Hexen-2 -one 98 C6H10O _ _____ 000109-49-9 7 Abundance Scan 289 (7.695 min): 26008.D (-) m/z 43.0.5 100.00% 43

5000 59

101 1 1 1 i 1 1 1 1 n 1 ■ 1 i 1 * 1 1 । 1 ' > ' 7.40 7.60 7.80 8.00

mz-> I " ‘11 m I" " r ■" i83■1" r ".111'" i" " i''" r " ■ i" " i' r " ■ i" I"1 • i"'111 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 207 m/z 59.05 47.23% Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- I 43

5000 59 7.40 7.60 7.80 8.00 101 m/z 101.05 21.55% 15 31 | . i . .I 83 I F" ‘ 'I ' i" " i1 ■" r "1 r " ■ i 11"11 ‘I ""I1‘"I ""I ' r "' r " ‘ i" " r " 'i"" r ,,,i" " i m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #3292: Acetic acid. 1,1-dimethylethyl ester 43

7.40 7.60 7.80 8.00 5000 - 57 m/z 58.05 18.84%- 101 15 27 " r "' iH " i" " r "' r "' I" " r "' i" " i' ■ ■' i" " r "' i" " r' m " " 11TT "111''" l11'' 11'1' I 1‘T miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 Abundance #1640: Morpholine, 4-methyl- 43 7.40 7.60 7.80 8.00 m/ z 41.00 7.19% 5000 - 101 15 71 I ..... 27 .... ... .... NN—vww) m/z-> ।... km 10 20 30 40 50 60 70 80 90 100110120130140150160170180 190 200 210 7.40 7.60 7.80 3.00

26008.D GCMS1126.M Wed Dec 12 09:51:58 2001 Page 2

NYC-WTC_000030873

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Gas chromatography-mass spectrometry scan record from late October to November 2001 regarding environmental sample analysis.

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