Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
NYC-WTC_000018287–000018315Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\JANI802\30986A.D Vial: 3 Acq On 18 Jan 2002 5:36 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclotetrasiloxane, octamethyl Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.
10.97 2.39 ug/1 910934 1,4-Dichlorobenzene-d4 11.49
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotet asiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 78 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 47 3 2-Oxo-4-phenyl-6- (4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 6,7 -Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 Abundance Scan 645 (10.968 min): 30986A.D (-) m/z 281.00 100.00% 281
5000 -
45 59 73 85 . 103 119 133 147 163 177 13207 221 235 249 265 ., Pr » i j r » l iT » »1 । i ) i I । T « I i | e » » i | 1 f i i j i • > T’t i « 1’ J | If" I IT‘I‘4‘‘‘‘I r"r4n 1‘ ! 1—7 10.60 10.80 11.00 11.20 rn/z 282.00 27.90% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
5000 । j » i । i i f i11' i j r T ] n i i j n 10.60 10.80 11.00 11.20 m/z 283.00 17.66% ! . ....... 7 133 ,,. .163 177.191 20 . . 235 249 285. _ 1 , miz-> 40 60 80 100/ 120 140 160 180 200 220 240 260 ' 280' Abundance #39643; Benzene, 1-phenyl-4-(2-cyano-2-phenyletheny!) 281 • i • * 10.60 10.80 11.00 11.20 5000 m/z 192.90 12.74% 253 126 203 1 266 ! ■ ■ i ■' • ■ । ■ I 224 240 -11111‘11r411111111111111111-711111110311313 1 * I dri ' 1 ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi ' II***IT‘ mm—" i i > i ] ■■■■ 281 10.60 10.80 11.00 11.20 m/z 133.00 11.06% 5000
1‘1‘01010—-09—102 H———123 141 175 204 247 | ntu——**———uonmwotutnnf miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.60 10.80 11.00 11.20 ' ‘ ‘ '
30986A.D GCMS1126.M Tue Jan 22 10:17:38 2002 Page 4
NYC-WTC_000018298
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018058
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NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
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NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
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NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
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NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder