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GCMS analysis results, sample AD23901, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23901 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067467–000067480

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23901.D Vial: 6 Acq On : 17 Oct 2001 6:11 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L A******************************************************************** Peak Number 3 Cyclotrisiloxane, hexamethyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 7.22 0.50 ug/1 50568 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 72 2 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 56 3 IH-Indol^ 5-methyl-2-phenyl- 207 C15H13N 013228-36-9 45 4 IH-Indole, 1-methyl-2-phenyl- 207 C15H13N 003558-24-5 38 Abundance / 238 (7?222 min): 23901 .dT) m/z 207.00 100.00%

K 207

5000

96 J ‘ ‘ ‘ ' I ‘ '

42 57 73 I 115 163 , 6.80 7.00 7.20 7.40 tIo I''" I'"' I m/z 208.00 20.49% •nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #27918: Cyclotristloxane, hexamethyi- 207

5000 6.80 7.00 7.20 7.40 7.60 "in/z 95.90 17.15% 15 191

20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 'Abundance #48300: Arsenous acid, tris(trimethylsity!) ester 207 6.80 7.00 7.20 7.40 7.TO 5000 m/z 209.00 12.25%

73 105 133 44 II 191 223239 327 "' I" " I'' p-rtv- T jtt+t ■ I" " I" p-tn ■n&-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #24654: IH-lndote, 5-methyk2-phenyl- 207 6.80 7.00 7.20 7.40 7.60 m/z 132.90 8711% 5000

■nfe-> ' to" ' "l6o' 1'40' 'lTO '246' 260 '2^' 3^ 6.TO 7.66 7.^ 7.^ 7.TO

23901.D NP101901.M Tue Oct 23 12:47:28 2001 Page 3

NYC-WTC_000067477

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NYC-WTC_000067477Source: NYC Law Department, mirrored locally

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